1,3-二苯氧基-2-丙醇合成路线 (共 35 条)
反应条件
2-tert-butylimino-2-diethylamino-1,3-dimethylperhydro-1,3,2-diazaphosphorine supported on polystyrene (PS-BEMP; PS = 200-400 mesh polystyryl with 2percent of divinylbenzene) T=60°C; 20 h; Neat (no solvent); regioselective reaction;
参考文献
Zvagulis, Artis; Bonollo, Simona; Lanari, Daniela; Pizzo, Ferdinando; Vaccaro, Luigi
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 14-15 p. 2489 - 2496
反应条件
1: phenol With sodium ethanolate in ethanol T=20°C; 0.25 h; 2: epichlorohydrin in ethanol T=20°C; 24 h; Reflux;
参考文献
Tomasic, Tihomir; Hajsek, David; Svajger, Urban; Luzar, Jernej; Obermajer, Natasa; Petit-Haertlein, Isabelle; Fieschi, Franck; Anderluh, Marko
European Journal of Medicinal Chemistry, 2014 , vol. 75, p. 308 - 326
反应条件
β-cyclodextrin in water; acetone T=60°C; 8 h;
参考文献
Surendra; Krishnaveni, N. Srilakshmi; Nageswar; Rao, K. Rama
Journal of Organic Chemistry, 2003 , vol. 68, # 12 p. 4994 - 4995
反应条件
potassium hydroxide in water; toluene
参考文献
US5426182 A1, ;
US5739378 A1, ;
US5488180 A1, ;
反应条件
β-cyclodextrin in water T=60°C; 8 h;
参考文献
Journal of Organic Chemistry, , vol. 76, # 6 p. 1883 - 1886
反应条件
potassium carbonate in N,N-dimethyl-formamide T=135°C; 8 h;
参考文献
Farhanullah; Ji Ram, Vishnu
Synlett, 2009 , # 14 p. 2265 - 2268
反应条件
caesium carbonate in acetonitrile Reflux;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 17, # 10 p. 3588 - 3594
反应条件
caesium carbonate in acetonitrile Reflux;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 17, # 10 p. 3588 - 3594
参考文献
Journal of the American Chemical Society, , vol. 51, p. 3393