1: With triethylamine in acetonitrile 2 h; Reflux; 2: With sodium carbonate in water

暂无反应条件数据

1: With borane-THF in tetrahydrofuran T=20°C; 16 h; 2: With hydrogenchloride; water in tetrahydrofuran T=0°C; 0.5 h; Heating / reflux; 3: With sodium hydroxide; water in tetrahydrofuran T=20°C;

1: phenyllithium With 3-butyl-1,1-dimethyl-1,3-dihydro-benzo[c][1,2]oxasilole in tetrahydrofuran; anhydrous butyl ether T=-78 - 20°C; 1 h; Inert atmosphere; 2: 4-bromopyridine-2-carbonitrile With copper(l) iodide; dpca; palladium dichloride in tetrahydrofuran; anhydrous butyl ether T=20°C; 2 h; Inert atmosphere;

1: With sodium methylate in methanol T=20°C; 2: With ammonium chloride in methanol 2 h; Reflux;

1: borane-THF / tetrahydrofuran / 20 °C 2: 2 h / 100 °C 3: trifluoroacetic anhydride / dichloromethane / 1 h / 0 - 20 °C View Scheme