sodium hydride
1.) THF, 0.5 h, 2.) reflux, 6 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Brownbridge, Peter; Hunt, Paul G.; Warren, Stuart
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1695 - 1706
sodium hydride
1.) THF, 0.5 h, 2.) room temperature, 3 d; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Brownbridge, Peter; Hunt, Paul G.; Warren, Stuart
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1695 - 1706