3-甲酰基-2-丁烯酸乙酯合成路线 （共 46 条）
反应条件
manganese(IV) oxide in dichloromethane T=25°C; 1 h;
参考文献
Magoulas, George E.; Bariamis, Stavros E.; Athanassopoulos, Constantinos M.; Haskopoulos, Anastasios; Dedes, Petros G.; Krokidis, Marios G.; Karamanos, Nikos K.; Kletsas, Dimitris; Papaioannou, Dionissios; Maroulis, George
European Journal of Medicinal Chemistry, 2011 , vol. 46, # 2 p. 721 - 737
反应条件
hydrogenchloride in dichloromethane 1.5 h;
参考文献
Curley, Robert W.; Ticoras, Christ J.
Synthetic Communications, 1986 , vol. 16, # 6 p. 627 - 632
反应条件
sodium acetate in water; acetic acid 3.5 h; Heating;
参考文献
Le Baut; Sparfel; Clairc; et al.
European Journal of Medicinal Chemistry, 1983 , vol. 18, # 5 p. 447 - 455
反应条件
1: 90 percent / SeO2 / aq. ethanol / 24 h / Heating 2: 72 percent / CaSO4, MnO2 / CH2Cl2 / 1 h / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry, , vol. 51, # 2 p. 256 - 258
反应条件
sulfuric acid in water
参考文献
Le Baut; Sparfel; Clairc; et al.
European Journal of Medicinal Chemistry, 1983 , vol. 18, # 5 p. 447 - 455
反应条件
1: With sodium hydride in N,N-dimethyl-formamide T=0°C; 1 h; 2: With hydrogenchloride; water in dichloromethane T=20°C; 3 h;
参考文献
Steroids, , vol. 67, # 9 p. 789 - 798
参考文献
Journal of the American Chemical Society, , vol. 82, p. 2286 - 2288
反应条件
NaIO4 on SiO2 in dichloromethane T=20°C;
参考文献
Journal of the American Chemical Society, , vol. 135, # 5 p. 1816 - 1822
反应条件
1: hexamethylphosphoric amide / 2 h / Ambient temperature 2: 79 percent / activated MnO2 / CH2Cl2 / 3 h / Ambient temperature View Scheme
参考文献
Synthesis, , # 4 p. 297 - 300
