4,4’-二甲基二苯硫醚合成路线 (共 108 条)
反应条件
in dimethylsulfoxide-d6
T=110°C; 3 h; Inert atmosphere;
参考文献
Chen, Chaohuang; Weng, Zhiqiang; Hartwig, John F.
Organometallics, 2012 , vol. 31, # 22 p. 8031 - 8037
反应条件
in dimethyl sulfoxide
0.666667 h;
参考文献
Petrillo, Giovanni; Novi, Marino; Garbarino, Giacomo; Filiberti, Marcos
Tetrahedron Letters, 1988 , vol. 29, # 33 p. 4185 - 4188
参考文献
Hauptmann et al.
Justus Liebigs Annalen der Chemie, 1952 , vol. 576, p. 45,56
反应条件
sodium sulfide; water
参考文献
Purgotti
Gazzetta Chimica Italiana, 1890 , vol. 20, p. 30
反应条件
silver carbonate; palladium dichloride in ethyl acetate
T=120°C; 0.166667 h; Microwave irradiation; Catalytic behavior; Solvent;
参考文献
Li, Junchen; Bi, Xiaojing; Wang, Hongmei; Xiao, Junhua
RSC Advances, 2014 , vol. 4, # 37 p. 19214 - 19217
参考文献
Purgotti
Gazzetta Chimica Italiana, 1890 , vol. 20, p. 30
反应条件
T=240°C; 2 h; Further byproducts given;
参考文献
Gaber, Abd El-Aal M.; Atalla, Ahmed A.; Kamal El-Dean, Adel M.
Phosphorus, Sulfur and Silicon and Related Elements, 1996 , vol. 112, # 1-4 p. 131 - 136
反应条件
silver carbonate; palladium dichloride in dimethyl sulfoxide; N,N-dimethyl-formamide
T=120°C; 0.166667 h; Microwave irradiation; Catalytic behavior; SolventReagent/catalyst;
参考文献
Li, Junchen; Bi, Xiaojing; Wang, Hongmei; Xiao, Junhua
RSC Advances, 2014 , vol. 4, # 37 p. 19214 - 19217
反应条件
sodium isopropanolate in isopropyl alcohol
T=72°C; 23 h; var. of solvent, reagent, temp., time; D-incorporation into toluene; Product distributionMechanism;
参考文献
Chung, Sung-Kee; Sasamoto, Kazumi
Journal of the Chemical Society, Chemical Communications, 1981 , # 7 p. 346 - 347
反应条件
ethanethiol
T=600°C; 0.0138889 h; other reagents (hydrogensulfid), yield calculated on reacted comp.; Product distribution;
参考文献
Voronkov, M. G.; Deryagina, E. N.; Sukhomazova, E. N.
Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, # 4 p. 755 - 760
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 4 p. 846 - 850