N,N'-(对亚苯基)二甲苯胺合成路线 （共 10 条）
反应条件
sodium t-butanolate; palladium diacetate; bis(diphenylphosphinyl)ferrocene in toluene
T=100 - 110°C; 10.5 h;
参考文献
Hauck, Sheila I.; Lakshmi; Hartwig, John F.
Organic Letters, 1999 , vol. 1, # 13 p. 2057 - 2060
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; [Ni(OPh)3]2(dppf); sodium t-butanolate in toluene
T=60°C; 22 h; Schlenk techniqueInert atmosphere;
参考文献
Kampmann, Sven S.; Sobolev, Alexandre N.; Koutsantonis, George A.; Stewart, Scott G.
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 9 p. 1967 - 1973
反应条件
zinc(II) chloride
T=220°C;
参考文献
Hatschek; Zega
Journal fuer Praktische Chemie (Leipzig), 1886 , vol. <2>33, p. 224
反应条件
zinc(II) chloride
T=210°C;
参考文献
Calm
Chemische Berichte, 1883 , vol. 16, p. 2799
反应条件
in acetic acid
T=60°C; Reduction; condensation; addition; cyclization; 3 h; Further byproducts given;
参考文献
Burmistrov; Toropin; Galamai; Likussar; Michelic; Reiner; Schubert-Zilavec
Russian Journal of Organic Chemistry, 1996 , vol. 32, # 8 p. 1231 - 1232
反应条件
1: 290 - 300 °C / im geschlossenen Rohr
2: zinc chloride / 210 °C
View Scheme
参考文献
Calm
Chemische Berichte, 1883 , vol. 16, p. 2799
反应条件
1: 290 - 300 °C / im geschlossenen Rohr
2: zinc chloride / 210 °C
View Scheme
参考文献
Calm
Chemische Berichte, 1883 , vol. 16, p. 2799
参考文献
Hatschek; Zega
Journal fuer Praktische Chemie (Leipzig), 1886 , vol. <2>33, p. 224
参考文献
Hatschek; Zega
Journal fuer Praktische Chemie (Leipzig), 1886 , vol. <2>33, p. 224
参考文献
Calm
Chemische Berichte, 1883 , vol. 16, p. 2799
