(2S)-4-甲基-3,5-噁唑啉羧酸乙酯合成路线 （共 6 条）
反应条件
1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane; 1,8-diazabicyclo[5.4.0]undec-7-ene; copper(ll) bromide
参考文献
Provencal, David P.; Gardelli, Cristina; Lafontaine, Jennifer A.; Leahy, James W.
Tetrahedron Letters, 1995 , vol. 36, # 34 p. 6033 - 6036
反应条件
1: 41 percent / nickel peroxide / hexane / 2 h / Heating 2: 66 percent / aq. KOH / 1 h / Heating View Scheme
参考文献
Chattopadhyay, Shital K.; Kempson, James; McNeil, Alan; Pattenden, Gerald; Reader, Michael; Rippon, David E.; Waite, David
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 15 p. 2415 - 2428
反应条件
triethylamine in dichloromethane
T=25°C; Cyclization; Condensation;
参考文献
Chattopadhyay, Shital K.; Kempson, James; McNeil, Alan; Pattenden, Gerald; Reader, Michael; Rippon, David E.; Waite, David
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 15 p. 2415 - 2428
参考文献
Provencal, David P.; Gardelli, Cristina; Lafontaine, Jennifer A.; Leahy, James W.
Tetrahedron Letters, 1995 , vol. 36, # 34 p. 6033 - 6036
反应条件
triethyloxonium tetra-fluoroborate; triethylamine
1.) methylene chloride, RT, 20 h, 2.) methylene chloride, RT, 16 h; Yield given. Multistep reaction;
参考文献
Meyers, A. I.; Hanagan, Mary Ann; Mazzu, Arthur L.
Heterocycles, 1981 , vol. 15, # 1 p. 361 - 367
反应条件
1: 41 percent / nickel peroxide / hexane / 2 h / Heating
2: 66 percent / aq. KOH / 1 h / Heating
3: SOCl2 / 4 h / Heating
View Scheme
参考文献
Chattopadhyay, Shital K.; Kempson, James; McNeil, Alan; Pattenden, Gerald; Reader, Michael; Rippon, David E.; Waite, David
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 15 p. 2415 - 2428
