alpha,alpha-二溴-4-硝基甲苯合成路线 (共 28 条)
反应条件
1: aqueous NaOBr solution 2: SbF3 / 100 °C 3: tin (II)-chloride; aq.-ethanolic hydrochloric acid View Scheme
参考文献
Jones
Journal of the American Chemical Society, 1947 , vol. 69, p. 2352
反应条件
1: aqueous NaOBr solution 2: SbF3 / 100 °C 3: tin (II)-chloride; aq.-ethanolic hydrochloric acid 4: ueber die Diazonium-Verbindung 5: water; bromine 6: aq. NaOH solution View Scheme
参考文献
Jones
Journal of the American Chemical Society, 1947 , vol. 69, p. 2352
反应条件
1: aqueous NaOBr solution 2: SbF3 / 100 °C 3: tin (II)-chloride; aq.-ethanolic hydrochloric acid 4: Diazotization.Behandlung der Diazoniumsalz-Loesung mit KI View Scheme
参考文献
Jones
Journal of the American Chemical Society, 1947 , vol. 69, p. 2352
反应条件
1: aqueous NaOBr solution 2: SbF3 / 100 °C 3: tin (II)-chloride; aq.-ethanolic hydrochloric acid View Scheme
参考文献
Jones
Journal of the American Chemical Society, 1947 , vol. 69, p. 2352
反应条件
1: aqueous NaOBr solution 2: SbF3 / 100 °C 3: tin (II)-chloride; aq.-ethanolic hydrochloric acid 4: Diazotization.Behandlung der Diazoniumsalz-Loesung mit CuBr in wss. HBr View Scheme
参考文献
Jones
Journal of the American Chemical Society, 1947 , vol. 69, p. 2352
反应条件
1: aqueous NaOBr solution 2: SbF3 / 100 °C 3: tin (II)-chloride; aq.-ethanolic hydrochloric acid 4: ueber die Diazonium-Verbindung View Scheme
参考文献
Jones
Journal of the American Chemical Society, 1947 , vol. 69, p. 2352
反应条件
1: aqueous NaOBr solution 2: SbF3 / 100 °C View Scheme
参考文献
Jones
Journal of the American Chemical Society, 1947 , vol. 69, p. 2352
反应条件
sulfuric acid; water
参考文献
Eliel; Nelson
Journal of the Chemical Society, 1955 , p. 1628
反应条件
sodium tetrahydroborate in ethylene glycol dimethyl ether; water T=20°C; 1 h;
参考文献
WO2010/52536 A1, ;
Example 4 ;
参考文献
Zimmermann; Mueller
Chemische Berichte, 1884 , vol. 17, p. 2936