2-甲氧基-4-(2-硝基乙烯)酚合成路线 (共 14 条)
反应条件
aluminum oxide; potassium carbonate 0.0833333 h; microwave irradiation;
参考文献
Wang, Cunde; Wang, Song
Synthetic Communications, 2002 , vol. 32, # 22 p. 3481 - 3486
反应条件
ammonium formate; palladium on activated charcoal in ethanol 2 h; Ambient temperature;
参考文献
Kulikov, S. V.; Samartsev, M. A.
Journal of Organic Chemistry USSR (English Translation), 1992 , vol. 28, # 2.2 p. 280 - 288
Zhurnal Organicheskoi Khimii, 1992 , vol. 28, # 2 p. 348 - 358
反应条件
hydrogen bromide; trifluoroacetic acid T=90°C; 0.166667 h;
参考文献
Kulikov, S. V.; Samartsev, M. A.
Journal of Organic Chemistry USSR (English Translation), 1992 , vol. 28, # 2.2 p. 280 - 288
Zhurnal Organicheskoi Khimii, 1992 , vol. 28, # 2 p. 348 - 358
反应条件
1: 71 percent / KOH, tetrabutylammonium bromide / ethanol / 1 h / 0 °C 2: 85 percent / AcONa. Ac2O / 0.08 h / Heating 3: 58 percent / CF3COOH, 45 aq. HBr / 0.17 h / 90 °C View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 28, # 2.2 p. 280 - 288
Zhurnal Organicheskoi Khimii, , vol. 28, # 2 p. 348 - 358
反应条件
1: 100 percent / K2CO3, tetrabutylammonium bromide / dimethylformamide / 5 h / 18 - 20 °C 2: 71 percent / KOH, tetrabutylammonium bromide / ethanol / 1 h / 0 °C 3: 85 percent / AcONa. Ac2O / 0.08 h / Heating 4: 58 percent / CF3COOH, 45 aq. HBr / 0.17 h / 90 °C View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 28, # 2.2 p. 280 - 288
Zhurnal Organicheskoi Khimii, , vol. 28, # 2 p. 348 - 358
反应条件
sodium methylate Behandeln des Reaktionsproduktes mit Salzsaeure;
参考文献
DE247817 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 11, p. 1016
参考文献
Chemische Berichte, , vol. 37, p. 4508
参考文献
Chemische Berichte, , vol. 37, p. 4508
反应条件
diisobutylaluminium hydride in 1,4-dioxane T=60°C;
参考文献
Vinogradova, V. I.; Yunusov, M. S.; Kuchin, A. V.; Tolstikov, G. A.; Sagandykov, R. T.; et al.
Chemistry of Natural Compounds, 1990 , vol. 26, # 1 p. 54 - 59
Khimiya Prirodnykh Soedinenii, 1990 , # 1 p. 67 - 74
反应条件
hydrogenchloride; hydrogen; palladium on activated charcoal in ethanol T=0°C; P=760 Torr;
参考文献
Kohno; Sasao; Murahashi
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 4 p. 1252 - 1254