(S)-(+)-2-辛醇合成路线 (共 200 条)
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
参考文献
Iriye, Ryozo; Takai, Katsuki; Noguchi, Masakazu
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 2 p. 199 - 202
反应条件
alkylsulfatase from Rhodococcus ruber DSM 44541; tri-(hydroxymethyl)-methylamine in water T=20°C; pH=7.5; 120 h; Title compound not separated from byproducts;
参考文献
Angewandte Chemie - International Edition, , vol. 41, # 21 p. 4052 - 4054
反应条件
tri-n-butyl-tin hydride in dichloromethane T=18°C; 0.0333333 h; Inert atmospherePhotolysis; enantioselective reaction;
参考文献
Hartung, Jens; Kempter, Irina; Gottwald, Thomas; Schwarz, Michaela; Kneuer, Rainer
Tetrahedron Asymmetry, 2009 , vol. 20, # 18 p. 2097 - 2104
反应条件
sol-gel encapsulated Candida antarctica lipase SP 525 T=20°C; 17 h;
参考文献
Bioscience, biotechnology, and biochemistry, , vol. 66, # 1 p. 221 - 223
反应条件
tri-n-butyl-tin hydride in dichloromethane T=18°C; 0.416667 h; Inert atmospherePhotolysis; enantioselective reaction;
参考文献
Hartung, Jens; Kempter, Irina; Gottwald, Thomas; Schwarz, Michaela; Kneuer, Rainer
Tetrahedron Asymmetry, 2009 , vol. 20, # 18 p. 2097 - 2104
反应条件
Novozym 435; potassium tert-butylate; sodium carbonate; [2,3,4,5-Ph4(η5-C4CNH(i-Pr))]Ru(CO)2Cl in toluene T=25°C; 72 h;
参考文献
Journal of Organic Chemistry, , vol. 69, # 6 p. 1972 - 1977
反应条件
whole cells of Sulfolobus acidocaldarius DSM 639 in phosphate buffer T=20°C; pH=2 - 3; Microbiological reaction;
参考文献
Organic Letters, , vol. 6, # 26 p. 5009 - 5010
反应条件
2-(N-morpholino)ethanesulfonic acidbuffer; nicotinamide adenine dinucleotide; isopropyl alcohol T=30°C; 20 h; acetone powder of Geotrichum candidum;
参考文献
Nakamura; Matsuda
Journal of Organic Chemistry, 1998 , vol. 63, # 24 p. 8957 - 8964
反应条件
potassium phosphate; Novozym 435; (CO)2ClRu(benzyloxytetraphenylpentadienyl) in toluene T=20°C; 50 h;
参考文献
Organic Letters, , vol. 7, # 20 p. 4523 - 4526
反应条件
vinyl acetate in tetrachloromethane; acetone T=30°C; Resolution of racemateEnzymatic reaction; Thermodynamic data; SolventTime;
参考文献
Journal of Molecular Catalysis B: Enzymatic, , vol. 101, p. 23 - 27