(S)-(+)-2-辛醇合成路线 （共 200 条）
反应条件
1: With thionyl chloride in dichloromethane T=0°C; 1 h; Inert atmosphere; 2: With titanium tetrachloride in dichloromethane T=0°C; 0.5 h; Inert atmosphere; ConcentrationTemperatureTime; Overall yield = 90 percent;
参考文献
Mondal, Deboprosad; Li, Song Ye; Bellucci, Luca; Laino, Teodoro; Tafi, Andrea; Guccione, Salvatore; Lepore, Salvatore D.
Journal of Organic Chemistry, 2013 , vol. 78, # 5 p. 2118 - 2127
反应条件
hydrogenchloride T=100°C; levorotatory form of 2-chloro-octane;
参考文献
Pickard; Kenyon
Journal of the Chemical Society, 1911 , vol. 99, p. 55,71
Journal of the Chemical Society, 1914 , vol. 105, p. 1121,1123, 1128
反应条件
in pyridine; water; toluene
参考文献
Chisso Corporation
Patent: EP216530 B1, 1991 ;
反应条件
pyridine; toluene chlorocarbonic acid-<d-octyl-(2)>-ester;
参考文献
Hunter
Journal of the Chemical Society, 1924 , vol. 125, p. 1392
反应条件
dipotassium hydrogenphosphate; phosphoric acid; EC 1.1.1.2 ketoreductase in hexane T=25°C; pH=7.3; 168 h; Equilibrium constant; Further Variations:Solvents;
参考文献
Tewari, Yadu B.; Schantz, Michele M.; Phinney, Karen W.; Rozzell, J. David
Journal of Chemical Thermodynamics, 2005 , vol. 37, # 1 p. 89 - 96
反应条件
N-(1-chloro-2-methylprop-1-enyl)-N,N-dimethylamine in dichloromethane
1.) 0 deg C; 2.) rt., 3h;
参考文献
Munyemana, Francois; Frisque-Hesbain, Anne-Marie; Devos, Alain; Ghosez, Leon
Tetrahedron Letters, 1989 , vol. 30, # 23 p. 3077 - 3080
反应条件
hydrogenchloride; diethyl ether
参考文献
Cramer; Baldauf
Chemische Berichte, 1959 , vol. 92, p. 370,376
参考文献
Coe et al.
Journal of the Chemical Society, 1954 , p. 2281,2285
参考文献
Houssa; Phillips
Journal of the Chemical Society, 1932 , p. 111
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Gerrard
Journal of the Chemical Society, 1946 , p. 106,109
参考文献
Houssa; Phillips
Journal of the Chemical Society, 1932 , p. 111
Full Text Show Details
Brauns
Recueil des Travaux Chimiques des Pays-Bas, 1946 , vol. 65, p. 805
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Gerrard
Journal of the Chemical Society, 1944 , p. 86,88,1945 851
