2,4,6,8,10-环五硅氧烷合成路线 （共 11 条）
反应条件
1: T=33°C; P=3863.02 Torr; 2: With dodecylbenzenesulphonic acid in isopar P T=20°C; 3 h;
参考文献
WO2005/5441 A2, ;
Page/Page column 6; 7 ;
反应条件
water in diethyl ether; water addn. of (CH3)SiHCl2 to a mixt. of ether and crushed ice at -10 to 7°C under vigorous stirring;;
参考文献
US2595891 , ;
C. A., , p. 7821
反应条件
water in toluene T=20°C; 27 h;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 61, # 6.2 p. 1378 - 1383,1257 - 1261
反应条件
diethyl ether; d-N,a-dimethylphenethylamine
参考文献
Journal of the American Chemical Society, , vol. 68, p. 963
反应条件
water in toluene T=20°C; 27 h; Further byproducts given;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 61, # 6.2 p. 1378 - 1383,1257 - 1261
反应条件
hydrogenchloride in toluene T=20°C; 4 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 60, # 9.2 p. 2100 - 2106,1873 - 1878
反应条件
water in toluene T=20°C; 27 h; Further byproducts given;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 61, # 6.2 p. 1378 - 1383,1257 - 1261
反应条件
water in toluene T=20°C; 27 h; hydrolytic copolycondensation depending on final concentration of hydrochloric acid; other dialkyldichlorosilanes; Product distribution;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 61, # 6.2 p. 1378 - 1383,1257 - 1261
反应条件
tetrahydrofuran; lithium T=35 - 45°C; Product distributionMechanism;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 55, # 7 p. 1528 - 1533,1358 - 1362
参考文献
Journal of the American Chemical Society, , vol. 68, p. 963
