4,6-二硝基-1,3-二甲苯合成路线 （共 35 条）
反应条件
chromium(VI) oxide; sulfuric acid T=10 - 20°C;
参考文献
Zhang, Aimin; Han, Yaohua; Yamato, Kazuhiro; Zeng, Xiao Cheng; Gong, Bing
Organic Letters, 2006 , vol. 8, # 5 p. 803 - 806
反应条件
chromium(VI) oxide; sulfuric acid T=-10 - 20°C; 5 h;
参考文献
Havlik, Martin; Kral, Vladimir; Dolensky, Bohumil
Organic Letters, 2006 , vol. 8, # 21 p. 4867 - 4870
反应条件
palladium 10 on activated carbon; hydrogen in ethanol T=100°C; P=2585.81 Torr; 2 h; Inert atmosphere;
参考文献
Mousseau, James J.; Xing, Liyan; Tang, Nathalie; Cuccia, Louis A.
Chemistry - A European Journal, 2009 , vol. 15, # 39 p. 10030 - 10038
参考文献
Chang; Adams
Journal of the American Chemical Society, 1934 , vol. 56, p. 2089,2090
参考文献
Bavin
Canadian Journal of Chemistry, 1958 , vol. 36, p. 238
反应条件
ethanol; hydrogen sulfide; ammonia
参考文献
Beyerman; Wielaert
Recueil des Travaux Chimiques des Pays-Bas, 1952 , vol. 71, p. 1213,1218
反应条件
pyridine; hydrogen sulfide
参考文献
Jozkiewicz
Prace Wroclawsk.Towarz.nauk.<B>Chem.Abstr., 1956 , # 73 p. 5,32
Prace Wroclawsk.Towarz.nauk.<B>Chem.Abstr., 1958 , p. 3711
反应条件
1: NaHS; aqueous ethanol
2: aqueous hydrochloric acid; aqueous sodium nitrite solution / anschliessend Behandeln mit Kupfer(I)-chlorid und konz. wss. Salzsaeure
View Scheme
参考文献
Beyerman; Wielaert
Recueil des Travaux Chimiques des Pays-Bas, 1952 , vol. 71, p. 1213,1218
反应条件
2: 87 percent / FeSO4*7H2O, conc. HCl / H2O; ethanol; liquid ammonia / 1 h / 80 °C
3: 58 percent / 10percent KOH / ethanol / 3 h / 90 - 100 °C
View Scheme
参考文献
Quast, Helmut; Schoen, Norbert
Liebigs Annalen der Chemie, 1984 , # 1 p. 133 - 146
反应条件
2: 87 percent / FeSO4*7H2O, conc. HCl / H2O; ethanol; liquid ammonia / 1 h / 80 °C
3: 97 percent / 2 N NaOH / ethanol; H2O / 1) 80 deg C, 4 h, 2) 2 h, reflux
View Scheme
参考文献
Quast, Helmut; Schoen, Norbert
Liebigs Annalen der Chemie, 1984 , # 1 p. 133 - 146
