13,14-二羟基二十二烷酸合成路线 (共 13 条)
反应条件
sodium periodate; phosphoric acid; sodium carbonate
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 30, # 9 p. 865 - 866
反应条件
T=40°C; Geschwindigkeit der Oxydation;
参考文献
Doree; Pepper
Journal of the Chemical Society, 1942 , p. 481
参考文献
Monatshefte fuer Chemie, , vol. 38, p. 5
反应条件
1: 61.5 percent / aq. Na2CO3, H3PO4, NaIO4 2: 1.) NaH, DMSO View Scheme
参考文献
Subbaraman, A S; Mithran, S; Mamdapur, V R
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1991 , vol. 30, # 9 p. 865 - 866
反应条件
1: 89 percent / aq. Na2CO3, H3PO4, NaIO4 2: 1.) NaH, DMSO 3: PTS 4: 90 percent / LiAlH4 (LAH) / diethyl ether View Scheme
参考文献
Subbaraman, A S; Mithran, S; Mamdapur, V R
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1991 , vol. 30, # 9 p. 865 - 866
参考文献
Green; Hilditch
Journal of the Chemical Society, 1937 , p. 766
反应条件
1: LiAlH4 / diethyl ether 2: NaIO4 / ethanol 3: pyridine 4: H2 / Raney-Ni / ethanol View Scheme
参考文献
Dhekne,V.V. et al.
Journal of the Chemical Society, 1962 , p. 2348 - 2352
反应条件
1: (esterification) 2: aq. NaIO4 3: Py 4: H2 / Raney-Ni 5: KOH / ethanol View Scheme
参考文献
Dhekne,V.V. et al.
Indian Journal of Chemistry, 1966 , vol. 4, p. 524 - 526
反应条件
sodium periodate; phosphoric acid; sodium carbonate
参考文献
Subbaraman, A S; Mithran, S; Mamdapur, V R
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1991 , vol. 30, # 9 p. 865 - 866
反应条件
sodium periodate in chloroform; water
T=20°C; Oxidation; elimination; 6 h;
参考文献
Bieniarz, Christopher; Ramakrishna, Kornepati V.; Kelly, Terence P.
Journal of Labelled Compounds and Radiopharmaceuticals, 2000 , vol. 43, # 3 p. 243 - 250