乙基2,4-二甲基-3-糠酸酯合成路线 （共 20 条）
反应条件
1: 56 percent / acetic anhydride, trichloroacetic acid / toluene / Heating
2: 58 percent / m-chloroperbenzoic acid / CH2Cl2 / Ambient temperature
View Scheme
参考文献
Chan, Wing Hong; Lee, Albert W. M.; Chan, Eddy T. T.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 8 p. 945 - 946
反应条件
1: tributylphosphine / dichloromethane / 0.25 h / 20 °C
2: / acetic acid; N,N-dimethyl-formamide / 8 h / 60 °C / |Green chemistry
View Scheme
参考文献
Cao, Hua; Jiang, Huan-Feng; Zhou, Xiao-Song; Qi, Chao-Rong; Lin, Yuan-Guang; Wu, Jian-Yong; Liang, Qi-Mei
Green Chemistry, 2012 , vol. 14, # 10 p. 2710 - 2714
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride; toluene-4-sulfonic acid
1) benzene, 80 deg C, 1.5 h, 2) benzene, room temp., 15 min; Yield given. Multistep reaction;
参考文献
Srikrishna, A.; Krishnan, K.
Tetrahedron Letters, 1988 , vol. 29, # 39 p. 4995 - 4996
反应条件
ethanol; zinc(II) chloride
参考文献
Garcia Gonzalez et al.
Anales de la Real Sociedad Espanola de Fisica y Quimica, 1954 , vol. <B> 50, p. 407,412
反应条件
sodium tetrahydroborate; mercury(II) diacetate
1.) DMSO, 1 h, 2.) DMSO, 65 deg C, 48 h; Yield givenMultistep reaction;
参考文献
Badanyan; Chobanyan; Tirakyan; Danielyan
Chemistry of Heterocyclic Compounds, 1998 , vol. 34, # 7 p. 781 - 784
参考文献
Alexander; Baldwin
Journal of the American Chemical Society, 1951 , vol. 73, p. 356
参考文献
Akhmedov, Sh. T.; Sadykhov, N. S.; Ismailov, V. M.; Sadovaya, N. K.; Karimov, F. N.; Zefirov, N. S.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1984 , vol. 20, # 10 p. 1184
Khimiya Geterotsiklicheskikh Soedinenii, 1984 , vol. 20, # 10 p. 1428 - 1429
参考文献
Gonzalez et al.
Anales de la Real Sociedad Espanola de Fisica y Quimica, Serie B: Quimica, 1954 , vol. 50, p. 407,412
反应条件
1: 84 percent / aq. NaOH / 2 h / Heating
View Scheme
参考文献
Wenkert, Ernest; Khatuya, Haripada; Klein, Phillip S.
Tetrahedron Letters, 1999 , vol. 40, # 28 p. 5171 - 5174
反应条件
1: 85 percent / LiAlH4 / diethyl ether
2: 10 percent / boron trifluoride etherate / CHCl3
View Scheme
参考文献
Ichihara, Akitami; Nonaka, Masahiko; Sakamura, Sadao; Sato, Rinzo; Tajimi, Akitoshi
Chemistry Letters, 1988 , p. 27 - 30
