2-溴-N-甲基苯甲酰胺合成路线 （共 18 条）
反应条件
n-butyllithium in tetrahydrofuran T=-78°C; 2 h; Yields of byproduct given;
参考文献
Hendi, Mukta S.; Natalie, Kenneth J. Jr.; Hendi, Shivakumar B.; Campbell, James A.; Greenwood, Thomas D.; Wolfe, James F.
Tetrahedron Letters, 1989 , vol. 30, # 3 p. 275 - 278
反应条件
n-butyllithium in tetrahydrofuran T=-78°C; 2 h; Yields of byproduct given;
参考文献
Hendi, Mukta S.; Natalie, Kenneth J. Jr.; Hendi, Shivakumar B.; Campbell, James A.; Greenwood, Thomas D.; Wolfe, James F.
Tetrahedron Letters, 1989 , vol. 30, # 3 p. 275 - 278
反应条件
n-butyllithium in tetrahydrofuran T=-78°C; 2 h; Yields of byproduct given;
参考文献
Hendi, Mukta S.; Natalie, Kenneth J. Jr.; Hendi, Shivakumar B.; Campbell, James A.; Greenwood, Thomas D.; Wolfe, James F.
Tetrahedron Letters, 1989 , vol. 30, # 3 p. 275 - 278
反应条件
triethylamine in dichloromethane T=20°C; 2 h;
参考文献
Advanced Synthesis and Catalysis, , vol. 354, # 11-12 p. 2288 - 2300
反应条件
1: thionyl chloride / 2 h / Reflux 2: potassium carbonate / tetrahydrofuran / Cooling with ice View Scheme
参考文献
Chemical Communications, , vol. 47, # 44 p. 12074 - 12076
反应条件
potassium carbonate in tetrahydrofuran Cooling with ice;
参考文献
Chemical Communications, , vol. 47, # 44 p. 12074 - 12076
反应条件
thionyl chloride 2.) water; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 29, # 42 p. 5401 - 5404
反应条件
potassium dihydrogenphosphate; Cp*Rh(MeCN)3[ClO4]2; silver carbonate in 1,1-dimethylpropan-1-ol T=100°C; P=760.051 Torr; 24 h;
参考文献
Chemical Communications, , vol. 47, # 44 p. 12074 - 12076
反应条件
lithium aluminium tetrahydride; thionyl chloride 2.) THF, -15 deg C; Yield given. Multistep reaction;
参考文献
Ohkata, Katsuo; Ohnishi, Masako; Akiba, Kin-ya
Tetrahedron Letters, 1988 , vol. 29, # 42 p. 5401 - 5404
反应条件
1: With sulfur; [2,2']bipyridinyl; copper(l) iodide; potassium carbonate in 1-methyl-pyrrolidin-2-one
T=110°C; 24 h; Inert atmosphere;
2: With pyridine; N-methoxyamine hydrochloride in 1-methyl-pyrrolidin-2-one
T=110°C; 3 h; Inert atmosphere;
参考文献
Krasikova; Katkevics
Chemistry of Heterocyclic Compounds, 2013 , vol. 48, # 11 p. 1684 - 1690
Khim. Geterotsikl. Soedin., 2012 , vol. 48, # 11 p. 1800 - 1807
