2,2,7,7-四甲基-3,5-辛二炔合成路线 （共 34 条）
反应条件
potassium tert-butylate in pentane T=-50°C; 72 h;
参考文献
Tetrahedron, , vol. 50, # 6 p. 1707 - 1716
反应条件
[1,3-bis(diphenylphosphino) propane] dichloronickel(II) in tetrahydrofuran 1.) -78 deg C to r.t., 2.) r.t., 6 h;
参考文献
Liebigs Annales, , # 8 p. 1301 - 1311
反应条件
hydroxylamine hydrochloride; ethylamine; copper(l) chloride in tetrahydrofuran 1 h; Ambient temperature;
参考文献
Tetrahedron, , vol. 42, # 6 p. 1763 - 1768
反应条件
iron(III) chloride in tetrachloromethane; toluene T=25°C; 144 h; Product distribution;
参考文献
Bulletin de la Societe Chimique de France, , vol. 2, # 1-2 p. 16 - 20
反应条件
[1,3-bis(diphenylphosphino) propane] dichloronickel(II); 2,3-dichloro-1,3-butadiene in tetrahydrofuran 1.) -78 deg C to r.t., 2.) r.t., 6 h;
参考文献
Liebigs Annales, , # 8 p. 1301 - 1311
反应条件
1,4-dioxane; n-butyllithium; magnesium bromide; Cl2Ni(1,2-bis(diphenylphosphino)ethane) 24 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Liebigs Annalen, , # 3 p. 471 - 476
反应条件
in tetrahydrofuran -70 deg C to r.t.;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 11 p. 2892 - 2893
反应条件
potassium methanolate in methanol T=50°C; Yield given;
参考文献
Angewandte Chemie, , vol. 93, # 12 p. 1116 - 1117
反应条件
diethyl ether; nitrobenzene
参考文献
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, , vol. 42, p. 728
反应条件
trimethylphosphane 2.) reflux; Multistep reaction;
参考文献
Chemische Berichte, , vol. 122, p. 43 - 52
