(E)-3-(2-呋喃)丙烯腈合成路线 （共 27 条）
反应条件
sulfuric acid; nitric acid in acetic anhydride T=-20°C; 5 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Jaehnisch, K.; Seeboth, H.
Journal fuer Praktische Chemie (Leipzig), 1981 , vol. 323, # 1 p. 26 - 32
反应条件
sodium hydroxide; water
参考文献
Ried; Reitz
Chemische Berichte, 1956 , vol. 89, p. 2570,2573
反应条件
water; barium dihydroxide in 1,4-dioxane
T=70°C; 0.666667 h;
参考文献
Sinisterra, J. V.; Mouloungui, Z.; Delmas, M.; Gaset, A.
Synthesis, 1985 , # 12 p. 1097 - 1100
反应条件
tributylphosphine; zinc
T=100°C; 14 h; Yield given. Yields of byproduct given;
参考文献
Zheng, Jianhua; Yu, Yang; Shen, Yanchang
Synthetic Communications, 1990 , vol. 20, # 21 p. 3277 - 3282
反应条件
hydrogen azide; anhydrous magnesium perchlorate in chloroform
T=30 - 50°C; Schmidt reaction; 1.16667 h;
参考文献
Pavlov
Chemistry of Heterocyclic Compounds, 2001 , vol. 37, # 10 p. 1199 - 1202
反应条件
[(Me)PNP(i-Pr)]NiOTf; 1,8-diazabicyclo[5.4.0]undec-7-ene
T=22°C; 24 h;
参考文献
Fan, Lei; Ozerov, Oleg V.
Chemical Communications, 2005 , # 35 p. 4450 - 4452
反应条件
samarium; acetic acid in ethanol
T=20°C; 2 h;
参考文献
Guo; Zhang
Journal of Chemical Research - Part S, 2001 , # 1 p. 26 - 27
反应条件
Ru(1-iPr-3-μ-CHMeCH2-4,5-Me2-imidazol-2-yl)(PPh3)2(CO)H in toluene
T=70°C; indirect Wittig reaction; 2 h; Title compound not separated from byproducts;
参考文献
Burling, Suzanne; Paine, Belinda M.; Nama, Devendrababu; Brown, Victoria S.; Mahon, Mary F.; Prior, Timothy J.; Pregosin, Paul S.; Whittlesey, Michael K.; Williams, Jonathan M. J.
Journal of the American Chemical Society, 2007 , vol. 129, # 7 p. 1987 - 1995
反应条件
Cu(ClO4)2*6H2O; trimethylsilylazide; 2,3-dicyano-5,6-dichloro-p-benzoquinone in 1,2-dichloro-ethane
T=60°C; 2 h;
参考文献
Rokade, Balaji V.; Malekar, Sanjeev K.; Prabhu, Kandikere Ramaiah
Chemical Communications, 2012 , vol. 48, # 44 p. 5506 - 5508
反应条件
1-Hexylamine in pyridine; toluene
48 h; Heatingazeotropic water removal;
参考文献
Guyot, J.; Kergomard, A.
Tetrahedron, 1983 , vol. 39, # 7 p. 1167 - 1179
