1: With trifluorormethanesulfonic acid; magnesium sulfate in chlorobenzene T=100°C; Friedlaender type synthesis; 1.5 h; Inert atmosphere; 2: With potassium tert-butylate in chlorobenzene T=100°C; Friedlaender type synthesis; 0.166667 h; Inert atmosphere;
1: methyl iodide With Sn[N(SiMe3)2]2 in tetrahydrofuran T=20°C; 0.0833333 h; 2: With tetrabutyl ammonium fluoride in tetrahydrofuran T=20°C; 3: 3-(bromo)-quinoline With tris-(dibenzylideneacetone)dipalladium(0) in 1,4-dioxane 0.0333333 h; Heating; Further stages.;
Meth-Cohn, Otto; Rhouati, Salah; Tarnowski, Brian; Robinson, Andrew
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1537 - 1543
1: methyl iodide With Sn[N(SiMe3)2]2 in tetrahydrofuran T=20°C; 0.0833333 h; 2: With tetrabutyl ammonium fluoride in tetrahydrofuran T=20°C; 3: 3-(bromo)-quinoline With methyl-ethyl phosphite; tris-(dibenzylideneacetone)dipalladium(0) in 1,4-dioxane 0.0833333 h; Heating; Further stages.;