N,N-二甲基苯甲酰胺合成路线 （共 319 条）
反应条件
4-(N,N-dimethlyamino)pyridine in N,N-dimethyl-formamide T=-55°C; Substitution; 1 h;
参考文献
Journal of Organic Chemistry, , vol. 65, # 7 p. 2114 - 2121
反应条件
silica gel; triethylamine; p-toluenesulfonyl chloride T=20°C; 0.0166667 h;
参考文献
Khalafi-Nezhad, Ali; Parhami, Abolfath; Soltani Rad, Mohammad Navid; Zarea, Abdolkarim
Tetrahedron Letters, 2005 , vol. 46, # 40 p. 6879 - 6882
反应条件
in tetrahydrofuran LiNMe2/complex=5, Ar atm., room temp., 24 h; not isolated, detd. by gas chromy.;
参考文献
Journal of Organometallic Chemistry, , vol. 361, p. C37 - C40
反应条件
1: bromobenzene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; Negishi coupling reaction; 0.166667 h; Inert atmosphere; 2: With zinc(II) chloride in tetrahydrofuran; hexane T=-78 - 20°C; Negishi coupling reaction; Inert atmosphere; 3: 2-iodo-N,N-dimethylbenzamide With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran; hexane T=60°C; Negishi coupling reaction; 2 h; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 131, # 29 p. 10201 - 10210
反应条件
dysprosium T=20°C; 0.333333 h; Inert atmosphere;
参考文献
Chen, Weifeng; Li, Kebin; Hu, Ziqiang; Wang, Liliang; Lai, Guoqiao; Li, Zhifang
Organometallics, 2011 , vol. 30, # 7 p. 2026 - 2030
反应条件
tetrafluoroboric acid; benzoyl chloride in diethyl ether; dichloromethane T=20°C; 1 h;
参考文献
Boehme, Horst; Raude, Edgar
Chemische Berichte, 1981 , vol. 114, # 10 p. 3421 - 3429
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; oxygen in dimethyl sulfoxide 3 h;
参考文献
Yuste, Francisco; Origel, Alfredo E.; Brena, Leonardo J.
Synthesis, 1983 , # 2 p. 109 - 110
反应条件
pyridine; iodobenzene; carbon monoxide; bis(triphenylphosphine)palladium(II)-chloride T=140 - 145°C; P=4912.9 Torr;
参考文献
Journal of Organic Chemistry, , vol. 58, # 25 p. 7016 - 7021
反应条件
[hetba]Br; palladium (II) bromide in 1-methyl-pyrrolidin-2-one T=160°C; decarbonylative Heck olefination; 16 h;
参考文献
Angewandte Chemie - International Edition, , vol. 43, # 9 p. 1095 - 1098
反应条件
palladium diacetate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; trichlorophosphate T=135°C; 6 h; Inert atmosphere;
参考文献
Sawant, Dinesh N.; Wagh, Yogesh S.; Bhatte, Kushal D.; Bhanage, Bhalchandra M.
Journal of Organic Chemistry, 2011 , vol. 76, # 13 p. 5489 - 5494
