2,6-二甲基-5-庚烯-2-醇合成路线 (共 35 条)
参考文献
Justus Liebigs Annalen der Chemie, , vol. 675, p. 73 - 82
Bulletin de la Societe Chimique de France, , p. 658 - 660
Bulletin de la Societe Chimique de France, , p. 805 - 808
反应条件
magnesium in tetrahydrofuran
反应条件
in diethyl ether 1 h;
参考文献
Baskaran, Sundarababu; Islam, Imadul; Chandrasekaran, Srinivasan
Journal of Chemical Research, Miniprint, 1992 , p. 2213 - 2246
反应条件
1: 1.) sulfur trioxide pyridine complex, 2.) LiAlH4 / 1.) THF, 0 deg C, 5 h, 2.) THF 1 h, room temperature 2: 1.) m-CPBA, 2.) periodic acid / 2.) THF, 0 deg C, 3.) ether, 0 deg C View Scheme
参考文献
Tetrahedron, , vol. 50, # 22 p. 6505 - 6522
反应条件
1: 1.) sulfur trioxide pyridine complex, 2.) LiAlH4 / 1.) THF, 0 deg C, 5 h, 2.) THF, 1 h, room temperature 2: 1.) m-CPBA, 2.) periodic acid / 2.) THF, 0 deg C, 3.) ether, 0 deg C View Scheme
参考文献
Tetrahedron, , vol. 50, # 22 p. 6505 - 6522
参考文献
Chemische Berichte, 16 Ref. <1883>,2285
Journal fuer Praktische Chemie (Leipzig), , vol. <2>27, p. 364,377
反应条件
periodic acid; 3-chloro-benzenecarboperoxoic acid 2.) THF, 0 deg C, 3.) ether, 0 deg C; Multistep reaction. Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 50, # 22 p. 6505 - 6522
反应条件
periodic acid; 3-chloro-benzenecarboperoxoic acid 2.) THF, 0 deg C, 3.) ether, 0 deg C; Multistep reaction. Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 50, # 22 p. 6505 - 6522
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2>27, p. 364,377
参考文献
Chemische Berichte, , vol. 35, p. 3184
Justus Liebigs Annalen der Chemie, , vol. 329, p. 169
Chemische Berichte, , vol. 38, p. 1504
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 128, p. 111
Chemische Berichte, , vol. 37, p. 845