1-甲基-1,2,4-三唑合成路线 (共 29 条)
反应条件
in acetonitrile T=45°C; 48 h; Inert atmosphere;
参考文献
Chemical Communications, , vol. 49, # 46 p. 5316 - 5318
反应条件
in acetonitrile T=80°C; 3 h;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 97, # 8-9 p. 573 - 598
反应条件
sodium methylate in methanol T=60°C; 20 h;
参考文献
Journal of Organic Chemistry, , vol. 67, # 26 p. 9340 - 9345
反应条件
methyl iodide in chloroform T=20°C; 48 h;
参考文献
Russian Journal of Organic Chemistry, , vol. 31, # 8 p. 1118 - 1121
Zhurnal Organicheskoi Khimii, , vol. 31, # 8 p. 1227 - 1230
反应条件
methyl iodide in dichloromethane T=20°C; 48 h;
参考文献
Russian Journal of Organic Chemistry, , vol. 31, # 8 p. 1118 - 1121
Zhurnal Organicheskoi Khimii, , vol. 31, # 8 p. 1227 - 1230
参考文献
Journal of the American Chemical Society, , vol. 120, # 35 p. 9100 - 9101
参考文献
Journal fuer Praktische Chemie - Practical Applications and Applied Chemistry (Germany), , vol. 342, # 7 p. 682 - 699
反应条件
sodium hydride 1.) acetonitrile, 0 deg C, 24 h, 2.) dichloromethane, a) from -25 to 20 deg C, 1 h, b) 20 deg C, 72 h; Yield given. Multistep reaction;
参考文献
Acta Chemica Scandinavica, , vol. 44, # 10 p. 1050 - 1057
反应条件
in chloroform T=20°C; 48 h;
参考文献
Russian Journal of Organic Chemistry, , vol. 31, # 8 p. 1118 - 1121
Zhurnal Organicheskoi Khimii, , vol. 31, # 8 p. 1227 - 1230
反应条件
in dichloromethane T=42°C; 3 h; Further byproducts given;
参考文献
Russian Journal of Organic Chemistry, , vol. 31, # 8 p. 1118 - 1121
Zhurnal Organicheskoi Khimii, , vol. 31, # 8 p. 1227 - 1230