2,4,6-三溴-1,3,5-三甲基苯合成路线 （共 18 条）
反应条件
1: 2,4,6-tribromomesitylene With bromine in dichloromethane 10 h; Heating; 2: potassium acetate in N,N-dimethyl-formamide T=80°C; 20 h; 3: With potassium hydroxide in water T=90°C; 22 h; Further stages.;
参考文献
Organic Letters, , vol. 5, # 4 p. 549 - 552
反应条件
1: With bromine in dichloromethane T=20°C; 0.5 h; sunlamp irradiation; 2: in dichloromethane 24 h; Heating; Further stages.;
参考文献
Bruns, Dirk; Miura, Hirokazu; Vollhardt, K. Peter C.; Stanger, Amnon
Organic Letters, 2003 , vol. 5, # 4 p. 549 - 552
反应条件
in N,N-dimethyl-formamide T=150 - 160°C; 8 h; Reflux;
参考文献
Achar, Tapas Kumar; Prakash, Ved; Biswal, Himansu S.; Mal, Prasenjit
Tetrahedron Letters, 2013 , vol. 54, # 9 p. 1067 - 1070
参考文献
LG ELECTRONICS INC.
Patent: EP1435384 A2, 2004 ;
反应条件
(i) Py, (ii) /BRN= 1948002/; Multistep reaction;
参考文献
Weis,C.D.
Journal of Organic Chemistry, 1962 , vol. 27, p. 2964 - 2965
反应条件
benzyltrimethylammonium bromide dibromide; zinc(II) chloride in acetic acid
T=70°C; 24 h;
参考文献
Kajigaeshi, Shoji; Kakinami, Takaaki; Moriwaki, Masayuki; Tanaka, Toshio; Fujisaki, Shizuo; Okamoto, Tsuyoshi
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 2 p. 439 - 443
反应条件
in tetrachloromethane
参考文献
LG ELECTRONICS INC.
Patent: EP1435384 A2, 2004 ;
参考文献
Smith; Moyle
Journal of the American Chemical Society, 1936 , vol. 58, p. 1,9
反应条件
Oxonereg;; quartz; sodium bromide in n-heptane
0.333333 h; Milling;
参考文献
Schmidt, Robert; Stolle, Achim; Ondruschka, Bernd
Green Chemistry, 2012 , vol. 14, # 6 p. 1673 - 1679
参考文献
Turowa-Poljak; Petrowa
Zhurnal Obshchei Khimii, 1946 , vol. 16, p. 829,830
Chem.Abstr., 1947 , p. 1621
