三乙氧基-[3-(3-三乙氧基硅烷基丙基硫基)丙基]硅烷合成路线 （共 17 条）
反应条件
1: TESPT With sodium in Solventreg; 140
T=110°C; 0.75 h;
2: octanoic acid chloride in Solventreg; 140
T=45 - 104°C; 1 h;
3: With water in toluene
T=45°C; Product distribution / selectivity;
参考文献
General Electric Company
Patent: US6777569 B1, 2004 ;
Location in patent: Page column 9 ;
反应条件
hydrogen sulfide; sodium in methanol
参考文献
Voronkov,M.G. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1977 , vol. 26, p. 1710 - 1713
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1977 , vol. 26, p. 1849 - 1851
反应条件
hydrogen sulfide
P=760 Torr; 2.5 h; Irradiation; Yield given;
参考文献
Maroshina, M.Yu.; Pozhidaev, Yu.N.; Palam, B.; Vlasova, N.N.; Voronkov, M.G.
Doklady Chemistry, 1994 , vol. 339, # 1-3 p. 205 - 207
Dokl. Akad. Nauk SSSR Ser. Khim., 1994 , vol. 339, # 1 p. 62 - 64
反应条件
sodium sulfide
T=-10 - 120°C; P=2400.24 Torr; 2 - 5.33333 h; Product distribution / selectivity;
参考文献
Degussa AG
Patent: EP1529782 A1, 2005 ;
Location in patent: Page/Page column 9; 10-11; 11; 11-12; ;
反应条件
sodium sulfide
T=50 - 102°C; 3 h; Product distribution / selectivity;
参考文献
Degussa AG
Patent: EP1529782 A1, 2005 ;
Location in patent: Page/Page column 10 ;
反应条件
sodium hydrogensulfide in ethanol
T=90 - 100°C; 2 - 4 h; Conversion of starting material;
参考文献
Degussa AG
Patent: EP1538152 A1, 2005 ;
Location in patent: Page/Page column 9; 10 ;
反应条件
sodium hydrogensulfide
T=90 - 100°C; 2 - 4 h; Conversion of starting material;
参考文献
Degussa AG
Patent: EP1538152 A1, 2005 ;
Location in patent: Page/Page column 10 ;
