1-(4-氯-苯基)-4-苯基-1,4-丁二酮合成路线 （共 15 条）
反应条件
zinc(II) chloride in tetrahydrofuran
T=40°C; 4 h;
参考文献
Yasuda, Makoto; Tsuji, Shoki; Shigeyoshi, Yusuke; Baba, Akio
Journal of the American Chemical Society, 2002 , vol. 124, # 25 p. 7440 - 7447
反应条件
sodium carbonate; triethylamine; 3,4-dimethyl-5-(2-hydroxyethyl)-thiazolium iodide in ethanol
T=80°C; 6 h;
参考文献
Stetter, Hermann; Jonas, Friedrich
Chemische Berichte, 1981 , vol. 114, # 2 p. 564 - 580
反应条件
1: diiodomethane With diethylzinc; trifluoroacetic acid in dichloromethane
T=0°C; 0.5 h;
2: 1-(4'-chlorophenyl)-3-phenylopropane-1,3-dione in dichloromethane
T=20°C; 5 h;
参考文献
Xue, Song; Li, Le-Zhen; Liu, Yong-Kang; Guo, Qing-Xiang
Journal of Organic Chemistry, 2006 , vol. 71, # 1 p. 215 - 218
反应条件
methanol; [RhCl(η2:η2-cycloocta-1,5-diene)]2; triphenylphosphine
T=80°C; P=15001.5 Torr; 18 h; AutoclaveInert atmosphere;
参考文献
Sauthier, Mathieu; Lamotte, Nicolas; Dheur, Julien; Castanet, Yves; Mortreux, Andre
New Journal of Chemistry, 2009 , vol. 33, # 5 p. 969 - 971
参考文献
Thorp; Brunskill
Journal of the American Chemical Society, 1915 , vol. 37, p. 1262
参考文献
Thorp; Brunskill
Journal of the American Chemical Society, 1915 , vol. 37, p. 1262
反应条件
1: alcohol
2: aqueous alcoholic KOH-solution
View Scheme
参考文献
Thorp; Brunskill
Journal of the American Chemical Society, 1915 , vol. 37, p. 1262
反应条件
1: alcohol
2: aqueous alcoholic KOH-solution
View Scheme
参考文献
Thorp; Brunskill
Journal of the American Chemical Society, 1915 , vol. 37, p. 1262
反应条件
1: CH2Cl2 / -78 °C
2: 42 percent Chromat. / CH2Cl2 / 0.17 h / Ambient temperature
View Scheme
参考文献
Zhdankin, Viktor V.; Mullikin, Michelle; Tykwinski, Rik; Berglund, Bruce; Caple, Ronald; et al.
Journal of Organic Chemistry, 1989 , vol. 54, # 11 p. 2605 - 2608
反应条件
in dichloromethane
0.166667 h; Ambient temperature;
参考文献
Zhdankin, Viktor V.; Mullikin, Michelle; Tykwinski, Rik; Berglund, Bruce; Caple, Ronald; et al.
Journal of Organic Chemistry, 1989 , vol. 54, # 11 p. 2605 - 2608
