tetrakis(triphenylphosphine) palladium(0); trimethylsilylazide; tetrabutyl ammonium fluoride in tetrahydrofuran
1 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
Rh6(CO)12; tetrabutyl-ammonium chloride; water; triethylamine in dimethyl sulfoxide
T=50°C; P=15200 Torr; 10 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Imada, Yasushi; Shibata, Ou; Murahashi, Shun-Ichi
Journal of Organometallic Chemistry, 1993 , vol. 451, # 1.2 p. 183 - 194