4-(苯基乙酰基)苯甲腈合成路线 （共 13 条）
反应条件
palladium diacetate; 1,4-di(diphenylphosphino)-butane in tetrahydrofuran T=90°C; P=1500.15 Torr; 1 h; Sealed tubeMicrowave irradiation; chemoselective reaction;
参考文献
Motwani, Hitesh V.; Larhed, Mats
European Journal of Organic Chemistry, 2013 , # 22 p. 4729 - 4733
反应条件
trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); 1,8-diazabicyclo[5.4.0]undec-7-ene; [(t-Bu)3PH]BF4 in tetrahydrofuran T=120°C; P=2250.23 Torr; 0.5 h; Microwave irradiationSealed tube; chemoselective reaction;
参考文献
European Journal of Organic Chemistry, , # 22 p. 4729 - 4733
反应条件
1,4-diaza-bicyclo[2.2.2]octane; water; oxygen in acetonitrile T=80°C; P=760.051 Torr; 12 h; chemoselective reaction;
参考文献
Su, Yijin; Sun, Xiang; Wu, Guolin; Jiao, Ning
Angewandte Chemie - International Edition, 2013 , vol. 52, # 37 p. 9808 - 9812
Angew. Chem., 2013 , p. 9990 - 9994
反应条件
1: 85 percent / acetic acid 2: sodium tert-butoxide / Pd2(dba)3; bis(2-diphenylphosphinophenyl)ether / dioxane / 24 h / 70 °C 3: 81.0 mg / aq. HCl / tetrahydrofuran; methanol / 16 h / 20 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 128, # 46 p. 14800 - 14801
反应条件
palladium diacetate; 1,4-di(diphenylphosphino)-butane; zinc in 1,4-dioxane T=100°C; Negishi coupling reaction; P=7500.75 Torr; 16 h; Inert atmosphereAutoclave;
参考文献
Chemistry - An Asian Journal, , vol. 7, # 1 p. 40 - 44
反应条件
1: AlCl3 / 3 h / 60 °C 2: dimethylsulfoxide / 120 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 113, # 25 p. 9640 - 9654
反应条件
palladium diacetate; 1,4-di(diphenylphosphino)-butane; zinc in 1,4-dioxane T=100°C; Negishi coupling reaction; P=7500.75 Torr; 16 h; Inert atmosphereAutoclave;
参考文献
Wu, Xiao-Feng; Schranck, Johannes; Neumann, Helfried; Beller, Matthias
Chemistry - An Asian Journal, 2012 , vol. 7, # 1 p. 40 - 44
反应条件
palladium diacetate; sodium t-butanolate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in toluene T=90°C; 5 h; Inert atmosphere;
参考文献
Cacchi, Sandro; Fabrizi, Giancarlo; Goggiamani, Antonella; Iazzetti, Antonia; Verdiglione, Rosanna
Synthesis (Germany), 2013 , vol. 45, # 12 art. no. SS-2013-Z0055-OP, p. 1701 - 1707
反应条件
1: AlCl3 / 3 h / 60 °C 2: dimethylsulfoxide / 120 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 113, # 25 p. 9640 - 9654
反应条件
1: AlCl3 2: dimethylformamide / Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 98, # 20 p. 6225 - 6233
