2,2-二乙氧基乙酸乙酯合成路线 (共 88 条)
反应条件
1: formyl formic acid in water T=70°C; P=37.5038 Torr; 2: ethanol With sulfuric acid in water Heating / reflux; Product distribution / selectivity;
参考文献
DSM FINE CHEMICALS AUSTRIA NFG GMBH and CO KG
Patent: WO2005/87711 A1, 2005 ;
Location in patent: Example 8 ;
反应条件
hydrogenchloride in ethanol
反应条件
N-ethyl-N,N-diisopropylamine in dichloromethane T=-10°C;
参考文献
Journal of Organic Chemistry, , vol. 46, # 12 p. 2557 - 2561
反应条件
Veresterung mit alkoh. Schwefelsaeure;
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 152, p. 960
Bulletin de la Societe Chimique de France, , vol. <4> 11, p. 539
反应条件
1: boron trifluoride etherate / CH2Cl2 / 1.) -30 deg C, 2.) 0 deg C, 15 min 2: 2 percent / i-Pr2EtN / CH2Cl2 / -10 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 46, # 12 p. 2557 - 2561
参考文献
Journal of Biological Chemistry, , vol. 26, p. 110
Journal of the American Chemical Society, , vol. 47, p. 3000
反应条件
pyridine; triethylamine in benzene
参考文献
Chemische Berichte, , vol. 95, p. 1832 - 1839
反应条件
hydrogenchloride 3 h; Heating;
参考文献
Sera, Akira; Itoh, Kuniaki; Yamada, Hiroshi; Aoki, Ryuichi
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 11 p. 3453 - 3455
参考文献
Chemische Berichte, , vol. 41, p. 3615
Biochemische Zeitschrift, , vol. 162, p. 488
参考文献
Journal of the Chemical Society, , p. 2679,2681