2-(2-溴乙氧基)苯甲醛合成路线 (共 10 条)
反应条件
potassium carbonate in N,N-dimethyl-formamide T=20°C; 72 h;
参考文献
Mizyed, Shehadeh A.; Ashram, Muhammad; Awwadi, Firas F.
Arkivoc, 2011 , vol. 2011, # 10 p. 277 - 286
反应条件
1: 2-methyl-benzyl alcohol With sodium hydroxide deprotonation; 2: ethylene dibromide Alkylation; 48 h; Heating;
参考文献
Fraga Dubreuil; Bazureau
Tetrahedron Letters, 2000 , vol. 41, # 38 p. 7351 - 7355
反应条件
potassium carbonate in acetonitrile 30 h; Heating;
参考文献
Ashram, Muhammad
Journal of the Chemical Society, Perkin Transactions 2, 2002 , # 10 p. 1662 - 1668
反应条件
potassium carbonate in acetonitrile 30 h; Heating;
参考文献
Ashram, Muhammad
Journal of the Chemical Society, Perkin Transactions 2, 2002 , # 10 p. 1662 - 1668
反应条件
in ethanol 16 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 53, # 22 p. 5272 - 5281
反应条件
T=130 - 140°C; im Druckrohr;
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2>77, p. 365
反应条件
1: 92 percent / tetrahydrofuran / 12 h / 65 °C 2: 92 percent / i-Pr2NEt; Bu3SnH; 1,1'-azobis(cyclohexanecarbonitrile) / tetrahydrofuran / 2 h / Heating View Scheme
参考文献
Clive, Derrick L. J.; Pham, Mai P.; Subedi, Rajendra
Journal of the American Chemical Society, 2007 , vol. 129, # 9 p. 2713 - 2717
反应条件
potassium tert-butylate in dimethyl sulfoxide 0.25 h; Ambient temperature;
参考文献
Kirmse, Wolfgang; Hoemberger, Guenter
Journal of the American Chemical Society, 1991 , vol. 113, # 10 p. 3925 - 3934
反应条件
1: 57 percent / potassium tert-butoxide / dimethylsulfoxide / 0.25 h / Ambient temperature 2: 85 percent / LiAlH4 / diethyl ether / 1 h / Heating View Scheme
参考文献
Kirmse, Wolfgang; Hoemberger, Guenter
Journal of the American Chemical Society, 1991 , vol. 113, # 10 p. 3925 - 3934
反应条件
potassium carbonate in acetonitrile
Inert atmosphereReflux;
参考文献
Mizyed, Shehadeh A.; Ashram, Muhammad; Awwadi, Firas F.
Arkivoc, 2011 , vol. 2011, # 10 p. 277 - 286