1,3,3-三苯基-1-丙酮合成路线 (共 136 条)
反应条件
anhydrous iron chloride in dichloromethane
T=60°C; 2 h;
参考文献
Yang, Cui-Feng; Wang, Jian-Yong; Tian, Shi-Kai
Chemical Communications, 2011 , vol. 47, # 29 p. 8343 - 8345
反应条件
phenyl-magnesium bromide in diethyl ether; benzene
0.25 h;
参考文献
Postnov, V. N.; Polivin, Yu. N.; Sazonova, V. A.; Grukhanova, S. N.
Journal of Organometallic Chemistry, 1985 , vol. 288, p. 197 - 200
反应条件
1: 4,4,5,5-tetramethyl-2-phenyl-[1,3,2]-dioxaborolane With diethylzinc in hexane; toluene
T=60°C; 12 h;
2: trans-1,3-diphenyl-2-propen-1-one in hexane; toluene
T=0°C; 10 h;
参考文献
Dong, Lin; Xu, Yan-Jun; Gong, Liu-Zhu; Mi, Ai-Qiao; Jiang, Yao-Zhong
Synthesis, 2004 , # 7 p. 1057 - 1061
反应条件
sodium methylate in methanol
参考文献
Yates,P.; Betts,M.J.
Journal of the American Chemical Society, 1972 , vol. 94, p. 1965 - 1970
反应条件
in tetrahydrofuran
T=-40°C; 0.666667 h;
参考文献
Sigalov, A. B.; Petrov, E. S.; Rybakova, L. F.; Beletskaya, I. P.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 11 p. 2351 - 2356
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 11 p. 2615 - 2620
反应条件
cerium(III) chloride in tetrahydrofuran
T=0°C; 1 h;
参考文献
Imamoto, Tsuneo; Takiyama, Nobuyuki; Nakamura, Kamikazu
Tetrahedron Letters, 1985 , vol. 26, # 39 p. 4763 - 4766
反应条件
in tetrahydrofuran
T=20°C; 3 h;
参考文献
Sigalov, A. B.; Petrov, E. S.; Rybakova, L. F.; Beletskaya, I. P.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 11 p. 2351 - 2356
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 11 p. 2615 - 2620
反应条件
iron(III) trifluoromethanesulfonate; butan-1-ol
T=120°C; Retro-Claisen condensation; 24 h; Neat (no solvent);
参考文献
Biswas, Srijit; Maiti, Sukhendu; Jana, Umasish
European Journal of Organic Chemistry, 2010 , # 15 p. 2861 - 2866
反应条件
HUSY-zeolite
T=130°C; 15 h; sealed tube;
参考文献
Sani Souna Sido, Abdelkarim; Chassaing, Stefan; Kumarraja, Mayilvasagam; Pale, Patrick; Sommer, Jean
Tetrahedron Letters, 2007 , vol. 48, # 33 p. 5911 - 5914
参考文献
Barre, Kohler
Journal of the American Chemical Society, 1928 , vol. 50, p. 2039