1,3,3-三苯基-1-丙酮合成路线 (共 136 条)
反应条件
methyl boronic acid; diethylzinc in toluene
T=0°C;
参考文献
Dong, Lin; Xu, Yan-Jun; Gong, Liu-Zhu; Mi, Ai-Qiao; Jiang, Yao-Zhong
Synthesis, 2004 , # 7 p. 1057 - 1061
反应条件
cerium(III) chloride in tetrahydrofuran; diethyl ether; cyclohexane
T=-78°C; 0.5 h;
参考文献
Imamoto, Tsuneo; Takiyama, Noboyuki; Nakamura, Kimikazu; Hatajima, Toshihiko; Kamiya, Yasuo
Journal of the American Chemical Society, 1989 , vol. 111, # 12 p. 4392 - 4398
反应条件
[Pd(1,2-bis(diphenylphosphanyl)ethane)(PhCN)2](SbF6)2; water in tetrahydrofuran
T=20°C; 23 h;
参考文献
Nishikata, Takashi; Yamamoto, Yasunori; Miyaura, Norio
Angewandte Chemie - International Edition, 2003 , vol. 42, # 24 p. 2768 - 2770
反应条件
anhydrous iron chloride in 1,2-dichloro-ethane
T=60°C; 1.5 h; regioselective reaction;
参考文献
Yang, Cui-Feng; Wang, Jian-Yong; Tian, Shi-Kai
Chemical Communications, 2011 , vol. 47, # 29 p. 8343 - 8345
反应条件
1: With [2,2']bipyridinyl; sodium acetate; copper(l) chloride in o-xylene
T=135°C;
2: With hydrogenchloride in o-xylene; water
参考文献
Liao, Yuan-Xi; Hu, Qiao-Sheng
Journal of Organic Chemistry, 2011 , vol. 76, # 18 p. 7602 - 7607
反应条件
tetrabutylammomium bromide; sodium hydrogencarbonate; palladium dichloride
T=120°C; Heck coupling; 36 h;
参考文献
Bouquillon, Sandrine; Ganchegui, Benjamin; Estrine, Boris; Henin, Francoise; Muzart, Jacques
Journal of Organometallic Chemistry, 2001 , vol. 634, # 2 p. 153 - 156
反应条件
di-tert-butyl peroxide; iron(II) chloride
T=100°C; 24 h; Inert atmosphere;
参考文献
Song, Chun-Xiao; Cai, Gui-Xin; Farrell, Thomas R.; Jiang, Zhong-Ping; Li, Hu; Gan, Liang-Bing; Shi, Zhang-Jie
Chemical Communications, 2009 , # 40 p. 6002 - 6004
反应条件
[Rh(OH)(cycloocta-1,5-diene)]2 in methanol
T=20°C; 2 h; Inert atmosphere;
参考文献
Matsuda, Takanori; Shiose, Shigeru; Suda, Yuya
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 1923 - 1926
反应条件
chloro-trimethyl-silane; [Cu(acetonitrile)2(triphenylphosphine)2](BF4) in diethyl ether
T=0°C; 1 h;
参考文献
Deshmukh; Jadhav, Sunil; Anbhule; Mali; Suryawanshi
Journal of Chemical Research, 2006 , # 4 p. 248 - 250
反应条件
anhydrous iron chloride in dichloromethane
T=60°C; 2 h;
参考文献
Yang, Cui-Feng; Wang, Jian-Yong; Tian, Shi-Kai
Chemical Communications, 2011 , vol. 47, # 29 p. 8343 - 8345