[(苯基甲基)亚氨基]二(亚甲基)]二膦酸合成路线 （共 6 条）
反应条件
hydrogenchloride; phosphoric acid
T=100 - 105°C; 2 h;
参考文献
Redmore, Derek; Dhawan, Balram
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 233 - 238
反应条件
tetraphosphorus hexa oxide; trifluorormethanesulfonic acid in acetonitrile
T=75°C; 3 h;
参考文献
STRAITMARK HOLDING AG; NOTTÉ, Patrick; COGELS, Samuel; BURCK, Sebastian
Patent: WO2014/12990 A1, 2014 ;
Location in patent: Page/Page column 24 ;
反应条件
hydrogenchloride in water
T=100°C; RefluxInert atmosphere;
参考文献
Prishchenko, Andrey A.; Livantsov, Mikhail V.; Novikova, Olga P.; Livantsova, Ludmila I.; Petrosyan, Valery S.
Heteroatom Chemistry, 2010 , vol. 21, # 6 p. 430 - 440
反应条件
1.1: hydrogenchloride / water / 100 °C / Reflux; Inert atmosphere
1.2: Reflux; Inert atmosphere
2.1: methanol; diethyl ether / 10 °C / Inert atmosphere
View Scheme
参考文献
Prishchenko, Andrey A.; Livantsov, Mikhail V.; Novikova, Olga P.; Livantsova, Ludmila I.; Petrosyan, Valery S.
Heteroatom Chemistry, 2010 , vol. 21, # 6 p. 430 - 440
反应条件
hydrogenchloride; orthophosphorus acid
参考文献
Moedritzer,K.; Irani,R.R.
Journal of Organic Chemistry, 1966 , vol. 31, p. 1603 - 1607
反应条件
water
1.) 130-140 deg C, 8 h; 2.) MeOH; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Issleib, Kurt; Balszuweit, Arno; Richter, Hans-Juergen; Tonk, Walter
Zeitschrift fuer Chemie (Stuttgart, Germany), 1983 , vol. 23, # 12 p. 434 - 436
