1-(2,2-二溴乙烯)-4-甲基苯合成路线 (共 23 条)
反应条件
water; zinc T=275°C; 4 h;
参考文献
Tetrahedron Letters, , vol. 44, # 25 p. 4685 - 4688
反应条件
samarium in methanol T=45°C; 6 h;
参考文献
Synlett, , # 8 p. 1137 - 1140
反应条件
lithium aluminium tetrahydride; ethyl acetate in tetrahydrofuran T=-40°C; 6 h;
参考文献
Synthesis, , # 7 p. 986 - 988
反应条件
samarium in methanol T=60°C; 6 h;
参考文献
Synlett, , # 8 p. 1137 - 1140
参考文献
Huh, Dal Ho; Ryu, Hoejin; Kim, Young Gyu
Tetrahedron, 2004 , vol. 60, # 44 p. 9857 - 9862
反应条件
anhydrous iron chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; acetylacetone in N,N-dimethyl-formamide T=125°C; 6 h;
参考文献
Zhao, Ming; Kuang, Chun Xiang; Cheng, Xue Zhi; Yang, Qing
Chinese Chemical Letters, 2011 , vol. 22, # 5 p. 571 - 574
反应条件
PEG-400; sodium hydroxide; bis[1,2-bis(diphenylphosphino)ethane]palladium(0) in dichloromethane T=60 - 65°C; 17 h;
参考文献
Li, Pei; Alper, Howard
Journal of Organic Chemistry, 1986 , vol. 51, # 23 p. 4354 - 4356
反应条件
caesium carbonate; dimethyl sulfoxide T=115°C; 12 h;
参考文献
Tetrahedron Letters, , vol. 52, # 9 p. 992 - 994
反应条件
potassium phosphate; copper(l) iodide; 8-hydroxy-quinoline in ethanol T=100°C; Suzuki Coupling; 12 h; Schlenk techniqueInert atmosphere;
参考文献
Liu, Jidan; Dai, Fenglin; Yang, Zhiyong; Wang, Sizhuo; Xie, Kai; Wang, Anwei; Chen, Xiang; Tan, Ze
Tetrahedron Letters, 2012 , vol. 53, # 42 p. 5678 - 5683
反应条件
triphenylphosphine in dichloromethane
T=0°C; 0.5 h;
参考文献
Huh, Dal Ho; Jeong, Ji Sang; Lee, Hee Bong; Ryu, Hoejin; Kim, Young Gyu
Tetrahedron, 2002 , vol. 58, # 50 p. 9925 - 9932