3-[[[(二甲基氨基)亚甲基]氨基]磺酰基]-5-硝基-4-苯氧基苯甲酸甲酯合成路线 （共 5 条）
参考文献
Hoechst Aktiengesellschaft
Patent: US4010273 A1, 1977 ;
反应条件
in acetonitrile
T=20°C;
参考文献
NEUROTHERAPEUTICS PHARMA, INC.; WANASKI, Stephen; COLLINS, Stephen; KINCAID, John
Patent: WO2012/18635 A2, 2012 ;
Location in patent: Page/Page column 111 ;
WO 2012/018635 A2
反应条件
1.1: sodium hydrogencarbonate / water / 85 °C
1.2: 20 °C
2.1: thionyl chloride / 50 °C
3.1: acetonitrile / 20 °C
View Scheme
参考文献
NEUROTHERAPEUTICS PHARMA, INC.; WANASKI, Stephen; COLLINS, Stephen; KINCAID, John
Patent: WO2012/18635 A2, 2012 ;
WO 2012/018635 A2
反应条件
1.1: sodium hydrogencarbonate / water / 85 °C
1.2: 20 °C
2.1: thionyl chloride / 50 °C
3.1: acetonitrile / 20 °C
View Scheme
参考文献
NEUROTHERAPEUTICS PHARMA, INC.; WANASKI, Stephen; COLLINS, Stephen; KINCAID, John
Patent: WO2012/18635 A2, 2012 ;
WO 2012/018635 A2
反应条件
1: thionyl chloride / 50 °C
2: acetonitrile / 20 °C
View Scheme
参考文献
NEUROTHERAPEUTICS PHARMA, INC.; WANASKI, Stephen; COLLINS, Stephen; KINCAID, John
Patent: WO2012/18635 A2, 2012 ;
WO 2012/018635 A2
Title/Abstract Full Text Show Details
NEUROTHERAPEUTICS PHARMA, INC.; WANASKI, Stephen, P.; COLLINS, Stephen, D.; KINCAID, John; DODSON, Gary, Steven
Patent: WO2013/59648 A1, 2013 ;
