(R)-(-)-2-庚醇合成路线 (共 33 条)
反应条件
Candida antarctica lipase B immobilized on acrylic resin catalyst in pentane T=20 - 25°C; 24 h; Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Strohalm, Hedwig; Dold, Susanne; Pendzialek, Kathrin; Weiher, Monika; Engel, Karl-Heinz
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 10 p. 6328 - 6333
反应条件
Candida antarctica lipase B immobilized on acrylic resin catalyst in pentane T=20 - 25°C; 24 h; Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Strohalm, Hedwig; Dold, Susanne; Pendzialek, Kathrin; Weiher, Monika; Engel, Karl-Heinz
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 10 p. 6328 - 6333
反应条件
Candida cylindracea lipase catalyst in n-heptane T=20 - 25°C; 24 h; Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Journal of Agricultural and Food Chemistry, , vol. 58, # 10 p. 6328 - 6333
反应条件
Candida antarctica lipase B immobilized on acrylic resin catalyst in pentane T=20 - 25°C; 24 h; Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Strohalm, Hedwig; Dold, Susanne; Pendzialek, Kathrin; Weiher, Monika; Engel, Karl-Heinz
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 10 p. 6328 - 6333
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Tetrahedron Letters, , vol. 37, # 46 p. 8379 - 8382
反应条件
lithium aluminium tetrahydride in diethyl ether 3 h; Ambient temperature;
参考文献
Tetrahedron Asymmetry, , vol. 9, # 2 p. 341 - 350
反应条件
(S)-2-(diphenylphosphino)-2'-methoxy-1,1'-binaphthyl; potassium fluoride; bis(η3-allyl-μ-chloropalladium(II)); trichlorosilane; hydrogen; dihydrogen peroxide; potassium hydrogencarbonate; palladium on activated charcoal Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 68, # 3 p. 713 - 722
反应条件
lyophilized cells of Rhodococcus ruber DSM 44541; acetone in phosphate buffer T=24°C; pH=8.0; 24 h; Title compound not separated from byproducts.;
参考文献
Journal of Organic Chemistry, , vol. 68, # 2 p. 402 - 406
反应条件
Candida antarctica lipase B immobilized on acrylic resin catalyst T=20 - 25°C; pH=7.4; 8 h; aq. phosphate bufferEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Journal of Agricultural and Food Chemistry, , vol. 58, # 10 p. 6328 - 6333
反应条件
Candida antarctica lipase B immobilized on acrylic resin catalyst T=20 - 25°C; pH=7.4; 8 h; aq. phosphate bufferEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Journal of Agricultural and Food Chemistry, , vol. 58, # 10 p. 6328 - 6333