1,2-二羟基-3-甲基蒽醌合成路线 （共 19 条）
反应条件
aluminium trichloride; sodium chloride
T=165°C; Fridel-Crafts acylation; 4 h;
参考文献
Dhananjeyan, Mugunthu R.; Milev, Youli P.; Kron, Michael A.; Nair, Muraleedharan G.
Journal of Medicinal Chemistry, 2005 , vol. 48, # 8 p. 2822 - 2830
反应条件
potassium carbonate
T=200°C;
参考文献
Baeyer; Fraude
Justus Liebigs Annalen der Chemie, 1880 , vol. 202, p. 163
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Fraude
Chemische Berichte, 1879 , vol. 12, p. 237
反应条件
aluminium trichloride; sodium chloride
T=165°C; 0.75 h;
参考文献
Zhang, Xiuguo; Fox, Brian W.; Hadfield, John A.
Synthetic Communications, 1996 , vol. 26, # 1 p. 49 - 62
反应条件
aluminium trichloride
T=200°C;
参考文献
Mitter; Pal
Journal of the Indian Chemical Society, 1930 , vol. 7, p. 259,261
反应条件
1: 97 percent / trimethylsilyl iodide / CHCl3 / 48 h / Ambient temperature
2: 32 percent / aluminum chloride, sodium chloride / 0.75 h / 165 °C
View Scheme
参考文献
Zhang, Xiuguo; Fox, Brian W.; Hadfield, John A.
Synthetic Communications, 1996 , vol. 26, # 1 p. 49 - 62
反应条件
sulfuric acid
T=260 - 270°C; Ueberfuehren der Sulfonsaeure in das Kaliumsalz und Erhitzen mit Kali auf 200grad;
参考文献
Fischer,O.
Chemische Berichte, 1875 , vol. 8, p. 675
反应条件
aluminium trichloride; sodium chloride
T=180 - 200°C;
参考文献
Lovie; Thomson
Journal of the Chemical Society, 1959 , p. 4139
反应条件
hydrogen bromide; acetic acid
参考文献
Janot et al.
Bulletin de la Societe Chimique de France, 1955 , p. 108,111
反应条件
1: concentrated sulfuric acid
2: potash / 200 °C
View Scheme
参考文献
Baeyer; Fraude
Justus Liebigs Annalen der Chemie, 1880 , vol. 202, p. 163
反应条件
1: concentrated sulfuric acid; KNO3
2: methanol
3: AlCl3 / 200 °C
View Scheme
参考文献
Mitter; Pal
Journal of the Indian Chemical Society, 1930 , vol. 7, p. 259,261
