反应条件
1.1: Mg; iodine / diethyl ether / 0 - 20 °C
1.2: 88 percent / diethyl ether; tetrahydrofuran / 20 °C
2.1: 86 percent / OsO4; N-methylmorpholine N-oxide / acetone; H2O; 2-methyl-propan-2-ol / 20 °C
3.1: 93 percent / NaIO4 / diethyl ether; H2O / 1 h
4.1: 91 percent / LiAlH4 / tetrahydrofuran / 0 °C
5.1: 56 percent / MnO2 / CHCl3 / 43 h / 20 °C
View Scheme
参考文献
Takikawa, Hirosato; Hosoe, Shintaro; Ueda, Keiko; Sasaki, Mitsuru
Bioscience, biotechnology, and biochemistry, 2004 , vol. 68, # 9 p. 1961 - 1965
