2-溴-2-甲基丙酸乙酯合成路线 (共 239 条)
反应条件
sulfuric acid; water
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2>33, p. 102
反应条件
pyridine in chloroform 1 h;
参考文献
Biochemical Pharmacology, , vol. 66, # 9 p. 1717 - 1726
Biochemical Pharmacology, , vol. 68, # 1 p. 185 - 193
反应条件
bromine 1.) irrad., reflux, 2.) 2 h; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 48, # 24 p. 4580 - 4582
参考文献
Journal of the American Chemical Society, , vol. 131, # 37 p. 13206 - 13207
反应条件
phosphorus; bromine Behandeln des erhaltenen Reaktionsprodukts mit Aethylalkohol;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 242, p. 161
Chemische Berichte, , vol. 24, p. 2218
Chemische Berichte, , vol. 34, p. 4044
参考文献
Journal of the American Pharmaceutical Association (1912-1977), , vol. 38, p. 599,601
Bulletin de la Societe Chimique de France, , p. 678,683
反应条件
potassium hydroxide 1) DMA, 100 deg C, 20 h; 2) MeOH, RT, 20 h; Yield given. Multistep reaction;
参考文献
Banzatti; Della Torre; Melloni; et al.
Journal of Heterocyclic Chemistry, 1983 , vol. 20, # 1 p. 139 - 144
反应条件
potassium hydroxide; zinc
参考文献
Rassow; Bauer
Chemische Berichte, 1908 , vol. 41, p. 965
Journal fuer Praktische Chemie (Leipzig), 1909 , vol. <2> 80, p. 100
参考文献
Idemitsu Kosan Company Limited
Patent: US5250686 A1, 1993 ;
反应条件
1: recorcinol With ethanol; sodium 1 h; Heating / reflux; 2: ethyl 2-bromo-2-methyl propionate in ethanol 3 h; Heating / reflux; 3: With water; acetic acid
参考文献
Pierre Fabre Medicament
Patent: US2008/167313 A1, 2008 ;
Location in patent: Page/Page column 15 ;