2-溴-2-丙烯-1-醇合成路线 （共 14 条）
反应条件
tetraethylammonium bromide; hydrogen bromide in dichloromethane T=25 - 45°C; 3 h;
参考文献
Snyder, Scott A.; Corey
Journal of the American Chemical Society, 2006 , vol. 128, # 3 p. 740 - 742
反应条件
Tetraethylammoniumhydroxid in dichloromethane T=40°C; 4 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Synthesis, , # 10 p. 805 - 806
反应条件
1: methylmalonic acid dimethyl ester With sodium hydride in tetrahydrofuran T=20°C; 2: 1-acetoxy-2-bromo-2-propene With tetrakis(triphenylphosphine) palladium(0); sodium methylate in tetrahydrofuran T=20°C; 2.5 h;
参考文献
Journal of Organic Chemistry, , vol. 68, # 10 p. 3918 - 3922
反应条件
1: methylmalonic acid dimethyl ester With sodium hydride in tetrahydrofuran T=20°C; 2: Carbonic acid 2-bromo-allyl ester ethyl ester With tetrakis(triphenylphosphine) palladium(0); sodium acetate in tetrahydrofuran T=20°C; 2.5 h;
参考文献
Journal of Organic Chemistry, , vol. 68, # 10 p. 3918 - 3922
反应条件
1: methylmalonic acid dimethyl ester With sodium hydride in tetrahydrofuran T=20°C; 2: 1-acetoxy-2-bromo-2-propene With tetrakis(triphenylphosphine) palladium(0); phenolated sodium in tetrahydrofuran T=20°C; 16 h;
参考文献
Journal of Organic Chemistry, , vol. 68, # 10 p. 3918 - 3922
参考文献
Chemische Berichte, , vol. 14, p. 404
Ann.scient.Brux.,
参考文献
Bulletin de la Societe Chimique de France, , p. 166
反应条件
toluene-4-sulfonic acid in benzene T=65°C; 18 h;
参考文献
Krafft, Marie E.
Tetrahedron Letters, 1986 , vol. 27, # 7 p. 771 - 774
反应条件
potassium hydroxide man Saettigt hierauf das Kali mit CO2,destilliert mit Wasser, scheidet aus dem Destillat den Alkohol durch K2CO3 ab und entwaessert ihn ueber K2CO3;
参考文献
Chemische Berichte, , vol. 14, p. 404
Ann.scient.Brux.,
Chemische Berichte, , vol. 5, p. 453,569
Chemische Berichte, , vol. 6, p. 729
参考文献
Chemische Berichte, , vol. 6, p. 729
