(9CI)-2,6-羟基-2-苯并噻唑羧酸乙酯合成路线 （共 12 条）
反应条件
sodium hydroxide in 1,4-dioxane
参考文献
Loewik, Dennis W. P. M.; Tisi, Lawrence C.; Murray, James A. H.; Lowe, Christopher R.
Synthesis, 2001 , # 12 p. 1780 - 1783
反应条件
1: 100 percent / aq. NaOH / dioxane 2: 74 percent / methanol / 60 °C View Scheme
参考文献
Synthesis, , # 12 p. 1780 - 1783
反应条件
1: Ethyl 6-hydroxybenzothiazole-2-carboxylate With potassium carbonate in N,N-dimethyl-formamide T=20°C; 0.5 h; 2: methyl iodide in N,N-dimethyl-formamide 1 h; Reflux;
参考文献
Meroni, Giuseppe; Rajabi, Mehdi; Ciana, Paolo; Maggi, Adriana; Santaniello, Enzo
Arkivoc, 2010 , vol. 2010, # 6 p. 53 - 60
反应条件
hydrogenchloride; water in ethanol
T=20°C; 24 h;
参考文献
Meroni, Giuseppe; Rajabi, Mehdi; Ciana, Paolo; Maggi, Adriana; Santaniello, Enzo
Arkivoc, 2010 , vol. 2010, # 6 p. 53 - 60
反应条件
1: in methanol
T=20°C; 1.5 h; Cooling with iceInert atmosphere;
2: With sodium hydroxide; potassium hexacyanoferrate(III) in water; isopropyl alcohol
T=20°C; 1 h; Inert atmosphereCooling with ice;
参考文献
Ciuffreda, Pierangela; Casati, Silvana; Meroni, Giuseppe; Santaniello, Enzo
Tetrahedron, 2013 , vol. 69, # 29 p. 5893 - 5897
反应条件
sodium hydroxide; potassium hexacyanoferrate(III) in water; isopropyl alcohol
T=20°C; 1.5 h;
参考文献
Meroni, Giuseppe; Rajabi, Mehdi; Ciana, Paolo; Maggi, Adriana; Santaniello, Enzo
Arkivoc, 2010 , vol. 2010, # 6 p. 53 - 60
反应条件
sodium hydroxide; potassium hexacyanoferrate(III) in water
T=20°C; 1 h;
参考文献
Meroni, Giuseppe; Rajabi, Mehdi; Ciana, Paolo; Maggi, Adriana; Santaniello, Enzo
Arkivoc, 2010 , vol. 2010, # 6 p. 53 - 60
反应条件
sodium hydroxide; potassium hexacyanoferrate(III) in water
T=20°C; 1 h;
参考文献
Meroni, Giuseppe; Rajabi, Mehdi; Ciana, Paolo; Maggi, Adriana; Santaniello, Enzo
Arkivoc, 2010 , vol. 2010, # 6 p. 53 - 60
反应条件
sodium hydroxide; potassium hexacyanoferrate(III) in ethanol
参考文献
McCapra,F.; Razavi,Z.
Journal of the Chemical Society, Chemical Communications, 1976 , p. 153 - 154
反应条件
sodium hydroxide; potassium hexacyanoferrate(III)
1 h;
参考文献
Loewik, Dennis W. P. M.; Tisi, Lawrence C.; Murray, James A. H.; Lowe, Christopher R.
Synthesis, 2001 , # 12 p. 1780 - 1783
