1-甲氧基-3-三甲基硅氧基-1,3-丁二烯合成路线 （共 15 条）
反应条件
triethylamine; lithium bromide in tetrahydrofuran 1) -15 deg C, 1 h; 2) 40 deg C, 24 h;
参考文献
Hansson, Lars; Carlson, Rolf
Acta Chemica Scandinavica, 1989 , vol. 43, # 2 p. 188 - 192
反应条件
sodium bromide 1.) DMF, room temperature, 20 min, 2.) room temperature, 8-10 h; Yield given. Multistep reaction;
参考文献
Synthetic Communications, , vol. 19, # 3and4 p. 515 - 522
反应条件
in dichloromethane T=50°C; P=7500600 Torr; 168 h; Yield given. Yields of byproduct given;
参考文献
Yamamoto, Yoshinori
Chemistry Letters, 1987 , p. 945 - 946
参考文献
Danishefsky; Harayama; Singh
Journal of the American Chemical Society, 1979 , vol. 101, # 23 p. 7008 - 7012
参考文献
Danishefsky; Harayama; Singh
Journal of the American Chemical Society, 1979 , vol. 101, # 23 p. 7008 - 7012
反应条件
in toluene T=130°C; 16 h;
参考文献
REATA PHARMACEUTICALS, INC.; O'BRIAN, Patrick, M.
Patent: WO2009/146218 A2, 2009 ;
Location in patent: Page/Page column 123 ;
反应条件
zinc(II) chloride in tetrahydrofuran; toluene T=20°C; 0.5 h;
参考文献
WO2013/130976 A1, ;
Paragraph 00287 ;
反应条件
zinc(II) chloride in tetrahydrofuran T=20°C; 72 h;
参考文献
US7115624 B1, ;
Page/Page column 85-87 ;
US 7115624 B1
参考文献
Journal of the American Chemical Society, , vol. 101, # 23 p. 7008 - 7012
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 38, # 7 p. 1832 - 1835
