2,3-二甲基-2-丁醇合成路线 (共 122 条)
参考文献
Wagner
Journal fuer Praktische Chemie (Leipzig), 1891 , vol. <2>44, p. 310
反应条件
1: aqueous H2SO4 2: AlCl3 View Scheme
参考文献
Wood,T.F. et al.
Journal of Organic Chemistry, 1963 , vol. 28, p. 2248 - 2255
反应条件
hydrogen bromide; bromine
参考文献
Stetter,H.; Tresper,E.
Chemische Berichte, 1971 , vol. 104, p. 71 - 74
反应条件
1: aqueous H2SO4 2: AlCl3 View Scheme
参考文献
Wood,T.F. et al.
Journal of Organic Chemistry, 1963 , vol. 28, p. 2248 - 2255
反应条件
ammonium hydroxide; sulfuric acid
1.) 80-85 deg.C, 2 h, 2.) H2O, 20 deg.C, 2,5 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yurovskaya, M. A.; Karchava, A. V.; Afanas'Ev, A. Z.; Bundel, Yu. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1992 , vol. 28, # 4 p. 409 - 413
Khimiya Geterotsiklicheskikh Soedinenii, 1992 , # 4 p. 489 - 494
反应条件
diethyl ether; methylmagnesium bromide
Man fuegt, nachdem Methan entwichen ist, Essigsaeureanhydrid zur aether. Loesung;
参考文献
Henry
Recueil des Travaux Chimiques des Pays-Bas, 1907 , vol. 26, p. 440
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1907 , vol. 144, p. 553 Anm.
Chem. Zentralbl., 1907 , vol. 78, # II p. 584
反应条件
potassium hydride
1.) THF, 2h, reflux, 2.) 1 h, reflux; Multistep reaction;
参考文献
Begtrup, Mikael
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , # 11 p. 1609 - 1618
参考文献
Delacre
Bulletin de la Societe Chimique de France, 1907 , vol. <4>1, p. 460
参考文献
Takahashi, Yukio; Yoneda, Norihiko
Synthetic Communications, 1989 , vol. 19, # 11-12 p. 1945 - 1954
反应条件
(i) K, benzene, (ii) /BRN= 473192/; Multistep reaction;
参考文献
Duismann,W. et al.
Justus Liebigs Annalen der Chemie, 1976 , p. 1820 - 1833