2,3-二甲基-2-丁醇合成路线 （共 122 条）
反应条件
methyl(trifluoromethyl)dioxirane in dichloromethane T=-22°C; 0.05 h;
参考文献
Journal of the American Chemical Society, , vol. 111, # 17 p. 6749 - 6757
反应条件
lithium aluminium tetrahydride; aluminium trichloride in diethyl ether 2 h; Ambient temperature;
参考文献
Synthesis, , # 11 p. 888 - 889
反应条件
2-hydroxy-1,3-isoindolinedione; air; anhydrous cobalt diacetate in benzonitrile T=100°C; Oxidation; P=7600 Torr; 8 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 71, # 5 p. 1237 - 1240
反应条件
1: With diborane in dichloromethane T=-16°C; hydroboration; 0.166667 h; 2: With dihydrogen peroxide in sodium hydroxide Oxidation;
参考文献
Tetrahedron Letters, , vol. 41, # 49 p. 9361 - 9364
反应条件
sodium tetrahydroborate in methanol T=25°C; 2 h; Title compound not separated from byproducts.;
参考文献
Journal of the American Chemical Society, , vol. 125, # 5 p. 1319 - 1328
反应条件
1: With n-butyllithium in tetrahydrofuran; hexane T=20°C; 2 h; Cooling with acetone-dry iceInert atmosphere; 2: With dihydrogen peroxide; sodium hydroxide in tetrahydrofuran; hexane; water T=0 - 20°C;
参考文献
Journal of Organic Chemistry, , vol. 78, # 7 p. 3057 - 3064
反应条件
1: With n-butyllithium in tetrahydrofuran; hexane T=20°C; 2 h; Cooling with acetone-dry iceInert atmosphere; 2: With dihydrogen peroxide; sodium hydroxide in tetrahydrofuran; hexane; water T=0 - 20°C;
参考文献
Journal of Organic Chemistry, , vol. 78, # 7 p. 3057 - 3064
反应条件
1: With n-butyllithium in tetrahydrofuran; hexane T=20°C; 2 h; Cooling with acetone-dry iceInert atmosphere; 2: With dihydrogen peroxide; sodium hydroxide in tetrahydrofuran; hexane; water T=0 - 20°C;
参考文献
Journal of Organic Chemistry, , vol. 78, # 7 p. 3057 - 3064
反应条件
iodosylbenzene; MnTTPPP(OAc) in benzene T=25°C; 7 h; other catalysts and regioselectivity investigated; Mechanism;
参考文献
Journal of the American Chemical Society, , vol. 108, # 23 p. 7281 - 7286
反应条件
chromium oxide-copper oxide barium oxide catalyst T=250°C; Hydrogenation.unter Druck;
参考文献
Journal of the American Chemical Society, , vol. 54, p. 4680
Nippon Kagaku Kaishi, , vol. 65, p. 141
Chem.Abstr., , p. 3757
