2,3,3-三甲基-1-丁烯合成路线 （共 91 条）
反应条件
hydrogenchloride; zinc(II) chloride
2.) ether, CH2Cl2, 20 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Mayr, Herbert; Klein, Herbert; Sippel, Elfriede
Chemische Berichte, 1983 , vol. 116, # 11 p. 3624 - 3630
反应条件
hydrogenchloride; zinc(II) chloride
2.) ether, CH2Cl2, -78 deg C, 24 h; Yield given. Multistep reaction. Title compound not separated from byproducts;
参考文献
Mayr, Herbert; Klein, Herbert; Sippel, Elfriede
Chemische Berichte, 1983 , vol. 116, # 11 p. 3624 - 3630
反应条件
hydrogenchloride; zinc oxide; zinc(II) chloride
2.) ether, CH2Cl2, 0 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Mayr, Herbert; Klein, Herbert; Sippel, Elfriede
Chemische Berichte, 1983 , vol. 116, # 11 p. 3624 - 3630
反应条件
hydrogenchloride; zinc oxide; zinc(II) chloride
2.) ether, CH2Cl2, 0 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Mayr, Herbert; Klein, Herbert; Sippel, Elfriede
Chemische Berichte, 1983 , vol. 116, # 11 p. 3624 - 3630
反应条件
1: 1.) conc. HCl, 2.) ZnCl2, ZnO / 2.) ether, CH2Cl2, -20 deg C, 4 h
2: ZnCl2, HCl / diethyl ether / 20 °C
3: 65 percent / Br2 / CCl4 / 2 h / Ambient temperature
View Scheme
参考文献
Mayr, Herbert; Klein, Herbert; Sippel, Elfriede
Chemische Berichte, 1983 , vol. 116, # 11 p. 3624 - 3630
反应条件
hydrogenchloride; zinc(II) chloride
2.) ether, CH2Cl2, -78 deg C, 24 h; Yield given. Multistep reaction. Title compound not separated from byproducts;
参考文献
Mayr, Herbert; Klein, Herbert; Sippel, Elfriede
Chemische Berichte, 1983 , vol. 116, # 11 p. 3624 - 3630
反应条件
hydrogenchloride
unter Druck;
参考文献
Arnett, Edward M.; Pienta, Norbert J.
Journal of the American Chemical Society, 1980 , vol. 102, # 10 p. 3329 - 3334
反应条件
chromium(VI) oxide; acetic acid
T=80°C;
参考文献
Chavanne; Lejeune
Bulletin des Societes Chimiques Belges, 1922 , vol. 31, p. 100
Chem. Zentralbl., 1922 , vol. 93, # III p. 241
反应条件
chromic acid; acetic acid
参考文献
Chavanne; Lejeune
Bulletin des Societes Chimiques Belges, 1922 , vol. 31, p. 100
Chem. Zentralbl., 1922 , vol. 93, # III p. 241
参考文献
Chavanne; Lejeune
Bulletin des Societes Chimiques Belges, 1922 , vol. 31, p. 100
Chem. Zentralbl., 1922 , vol. 93, # III p. 241
