2,3,3-三甲基-1-丁烯合成路线 （共 91 条）
反应条件
oxygen; ozone in tetrachloromethane T=77°C; Kinetics; Further Variations:TemperaturesReaction partners;
参考文献
Helvetica Chimica Acta, , vol. 83, # 12 p. 3312 - 3332
反应条件
Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Burgess, Kevin; Ohlmeyer, Michael J.
Journal of Organic Chemistry, 1988 , vol. 53, # 21 p. 5178 - 5179
反应条件
[Ti(tert-butoxide)4]; oxygen; 5,15,10,20-tetraphenylporphyrin; (+)-Weinsaeure-diethylester Irradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Adam, Waldemar; Griesbeck, Axel; Staab, Eugen
Tetrahedron Letters, 1986 , vol. 27, # 25 p. 2839 - 2842
反应条件
sulphur(VI) hexafluoride in gas T=20°C; P=5 Torr; Irradiationgas phase photolysis in the absence of oxygen; Product distributionMechanism;
参考文献
Deslauriers, Helene; Collin, Guy J.
Canadian Journal of Chemistry, 1985 , vol. 63, p. 3168 - 3173
反应条件
hydrogen; triethylamine; (PPh3)3Rh(CO)Cl in benzene
P=76000 Torr; 24 h;
参考文献
Azzena, Ugo; Luisi, Pier Luigi; Suter, Ulrich W.; Gladiali, Serafino
Helvetica Chimica Acta, 1981 , vol. 64, # 8 p. 2821 - 2829
参考文献
Quast, Helmut; Frank, Rolf; Heublein, Alfred; Schmitt, Edeltraud
Liebigs Annalen der Chemie, 1980 , # 11 p. 1814 - 1835
反应条件
P=0.4 Torr; Irradiation; Rate constant;
参考文献
Nakashima, Nobuaki; Shimo, Nobuo; Ikeda, Noriaki; Yoshihara, Keitaro
Journal of Chemical Physics, 1984 , vol. 81, # 8 p. 3738 - 3739
反应条件
zinc(II) chloride in diethyl ether; dichloromethane
T=-78°C;
参考文献
Klein, Herbert; Erbe, Anne; Mayr, Herbert
Angewandte Chemie, 1982 , vol. 94, # 1 p. 63
反应条件
hydrogenchloride; zinc(II) chloride
2.) ether, CH2Cl2, -78 deg C, 24 h; Yield given. Multistep reaction. Title compound not separated from byproducts;
参考文献
Mayr, Herbert; Klein, Herbert; Sippel, Elfriede
Chemische Berichte, 1983 , vol. 116, # 11 p. 3624 - 3630
反应条件
1: 1.) conc. HCl, 2.) ZnCl2, ZnO / 2.) ether, CH2Cl2, -20 deg C, 4 h
2: ZnCl2, HCl / diethyl ether / 20 °C
View Scheme
参考文献
Mayr, Herbert; Klein, Herbert; Sippel, Elfriede
Chemische Berichte, 1983 , vol. 116, # 11 p. 3624 - 3630
