2,3,3-三甲基-1-丁烯合成路线 (共 91 条)
反应条件
hypophosphorous ether; isopropyl alcohol; zinc(II) iodide in water T=150 - 200°C; 3 - 66 h; Product distribution / selectivity;
参考文献
WO2008/24896 A2, ;
Page/Page column 15-18 ;
反应条件
naphthalene-2-sulphonic acid
参考文献
Bl.Tokyo Inst.Technol.Chem.Abstr., , vol. 13, # 1 p. 1,4
Bl.Tokyo Inst.Technol.Chem.Abstr., , p. 3874
反应条件
isopropyl alcohol; phosphorous acid trimethyl ester; zinc(II) iodide T=175 - 200°C; 2 - 24 h; Product distribution / selectivity;
参考文献
WO2008/24896 A2, ;
Page/Page column 11-15 ;
反应条件
H-BEA T=199.84°C; P=465.047 Torr; Inert atmosphere;
参考文献
Angewandte Chemie, International Edition, , vol. 48, p. 3814 - 3816
Angewandte Chemie, , vol. 121, p. 3872 - 3874
反应条件
isopropyl alcohol; zinc(II) iodide T=200°C; 2 - 3 h;
参考文献
WO2008/24896 A2, ;
Page/Page column 19-20; 25-26 ;
反应条件
phosphoric acid in diethyl ether 3 h; Heating;
参考文献
Schwesinger, Reinhard; Willaredt, Juergen; Schlemper, Helmut; Keller, Manfred; Schmitt, Dieter; Fritz, Hans
Chemische Berichte, 1994 , vol. 127, # 12 p. 2435 - 2454
反应条件
in diethyl ether 1.) 0 deg C, 2.) 25 deg C, 6h;
参考文献
House, Herbert O.; Gaa, Peter, C.; Lee, Joseph H. C.; VanDerveer, Don
Journal of Organic Chemistry, 1983 , vol. 48, # 10 p. 1670 - 1678
反应条件
Ru(CO)4I2 T=160°C; 3 h; Sealed tube;
参考文献
EP1900714 A1, ;
Page/Page column 4-6 ;
参考文献
Journal of the American Chemical Society, , vol. 90, p. 2082 - 2096
反应条件
in diethyl ether 1.5 h; Heating;
参考文献
Quast, Helmut; Frank, Rolf; Heublein, Alfred; Schmitt, Edeltraud
Liebigs Annalen der Chemie, 1980 , # 11 p. 1814 - 1835