1: 1,1-Diiodoethane With zinc; PbCl2 in tetrahydrofuran
T=25°C; 1 h;
2: 4-lt;4-Nitro-phenylgt;-thiohydrocinnamat With trifuran-2-yl-phosphane; tris(dibenzylideneacetone)dipalladium (0) in tetrahydrofuran
T=0°C; 0.25 h;
3: chloro-trimethyl-silane in tetrahydrofuran
T=25°C; 6 h; Further stages.;
参考文献
Ooguri, Akihiro; Ikeda, Zenichi; Matsubara, Seijiro
Chemical Communications, 2007 , # 45 p. 4761 - 4763