in neat (no solvent) thermal decomposition of Hg(CH3)2 in presence of O2 and He as carrier gas;; mass spectroscopy;;
参考文献
Ingold; Bryce
Journal of Chemical Physics, 1956 , vol. 24, p. 360
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Gmelin Handbook: O: MVol.8, 35, page 2605 - 2607
in gas other Radiation; radio frequency radiation of mixt. of educts in a special pyrex reactor,ratio of educts: C2F6/alkyl metal = 25/1, 2h, condensation of product on a liquid N2 filled cold finger, excess C2F6 removed by vac. distn. at -100°C; sepn. by gas chromy. (10percent SE-30 on Chromosorb P);
