4-甲氧基-3-丙氧基苯甲醛合成路线 （共 8 条）
参考文献
Yakugaku Zasshi, , vol. 55, p. 1283,1285; engl. Ref. S. 244, 245
Chem.Abstr., , p. 2572
反应条件
potassium carbonate in N,N-dimethyl-formamide
参考文献
WO2007/25897 A2, ;
Page/Page column 105-106 ;
WO 2007/025897 A2
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene 1 h; Heating;
参考文献
Tetrahedron Letters, , vol. 34, # 14 p. 2343 - 2346
反应条件
1: K2CO3, 18-crown-6 / acetone / Heating 2: 70 percent / Bu3SnH, AIBN / benzene / 1 h / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 34, # 14 p. 2343 - 2346
反应条件
1: potassium carbonate; potassium iodide / ethanol / 10 h / |Reflux 2: trichlorophosphate / 19 h / 100 - 115 °C / |Cooling with ice View Scheme
参考文献
Research on Chemical Intermediates, , vol. 39, # 6 p. 2849 - 2856
反应条件
trichlorophosphate T=100 - 115°C; Vilsmeier-Haack Formylation; 19 h; Cooling with ice; Overall yield = 81.8 percent; Overall yield = 6.3 g;
参考文献
Research on Chemical Intermediates, , vol. 39, # 6 p. 2849 - 2856
反应条件
AlCl3, aluminium chloride in dichloromethane T=20°C; 5 h;
参考文献
Huang, Wei-Bin; Du, Cai-Yan; Jiang, Jian-An; Ji, Ya-Fei
Research on Chemical Intermediates, 2013 , vol. 39, # 6 p. 2849 - 2856
反应条件
sodium chlorite; aminosulfonic acid; acetic acid
1 h; Ambient temperature;
参考文献
Ashton, Michael J.; Cook, David C.; Fenton, Garry; Karlsson, Jan-Anders; Palfreyman, Malcolm N.; et al.
Journal of Medicinal Chemistry, 1994 , vol. 37, # 11 p. 1696 - 1703
