(6CI,7CI)-p-2-萘苯甲醚合成路线 （共 71 条）
反应条件
potassium carbonate; [PS-PEG-adppp-Pd(η3-C3H5)]Cl in water
T=50°C; Suzuki-Miyaura coupling; 12 h;
参考文献
Zhao, Chao-Wei; Ma, Jian-Ping; Liu, Qi-Kui; Yu, Yang; Wang, Peng; Li, Yan-An; Wang, Kui; Dong, Yu-Bin
Green Chemistry, 2013 , vol. 15, # 11 p. 3150 - 3154
反应条件
trans-chloro(9-phenanthrenyl)bis(triphenylphosphine)nickel(II); potassium carbonate; triphenylphosphine in toluene
T=110°C; Suzuki-Miyaura Coupling; 18 h; Inert atmosphere;
参考文献
Lei, Xiangyang; Obregon, Karla A.; Alla, Jhansi
Applied Organometallic Chemistry, 2013 , vol. 27, # 7 p. 419 - 424
反应条件
lithium chloride in tetrahydrofuran; toluene
T=110°C; 48 h; Inert atmosphere;
参考文献
Shirakawa, Eiji; Okura, Keisho; Uchiyama, Nanase; Murakami, Takuya; Hayashi, Tamio
Chemistry Letters, 2014 , vol. 43, # 6 p. 922 - 924
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran
T=20°C; Suzuki-Miyaura coupling; 8 h;
参考文献
Tang, Zhen-Yu; Hu, Qiao-Sheng
Journal of the American Chemical Society, 2004 , vol. 126, # 10 p. 3058 - 3059
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; (9-phenanthrenyl)Ni(II)(PPh3)2Cl; potassium carbonate in toluene
T=110°C; Suzuki Coupling; 30 h; Inert atmosphere;
参考文献
Hu, Feng; Lei, Xiangyang
Tetrahedron, 2014 , vol. 70, # 25 p. 3854 - 3858
反应条件
tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine in tetrahydrofuran; toluene
T=20°C; 1 h; Schlenk techniqueInert atmosphere;
参考文献
Giannerini, Massimo; Fananas-Mastral, Martin; Feringa, Ben L.
Nature Chemistry, 2013 , vol. 5, # 8 p. 667 - 672
反应条件
bis-triphenylphosphine-palladium(II) chloride; sodium lauryl sulfate; potassium carbonate; p-toluenesulfonyl chloride in water
T=60°C; Suzuki Coupling;
参考文献
Liu, Jin-Biao; Zhou, He-Ping; Peng, Yi-Yuan
Tetrahedron Letters, 2014 , vol. 55, # 17 p. 2872 - 2875
反应条件
potassium phosphate; NiCl2((PPh3)P)2 in toluene
T=110°C; 24 h; Inert atmosphere;
参考文献
Quasdorf, Kyle W.; Tian, Xia; Garg, Neil K.
Journal of the American Chemical Society, 2008 , vol. 130, # 44 p. 14422 - 14423
反应条件
bis(1,5-cyclooctadiene)nickel (0); cesium fluoride; tri-cyclo-hexyl-phosphine in toluene
T=120°C; Suzuki-Miyaura coupling; 12 h;
参考文献
Tobisu, Mamoru; Shimasaki, Toshiaki; Chatani, Naoto
Angewandte Chemie - International Edition, 2008 , vol. 47, # 26 p. 4866 - 4869
反应条件
1: 1-bromo-4-methoxy-benzene With tert.-butyl lithium in tetrahydrofuran; pentane
T=-78 - 20°C; Inert atmosphere;
2: With zinc(II) chloride in tetrahydrofuran; pentane
T=0 - 20°C; Inert atmosphere;
3: 2-naphthyl 2,2,2-trimethylacetate With Ni(PCy3)2Cl2 in tetrahydrofuran; N,N-dimethyl acetamide; pentane
T=70°C; 3 h; Inert atmosphere;
参考文献
Li, Bi-Jie; Li, Yi-Zhou; Lu, Xing-Yu; Liu, Jia; Guan, Bing-Tao; Shi, Zhang-Jie
Angewandte Chemie - International Edition, 2008 , vol. 47, # 52 p. 10124 - 10127
